Simple Method for Fatty Acids Determination in Food, Superfood and Spice Samples by GC-MS Technique

1. AOAC Guidelines for single laboratory validation of chemical methods for dietary supplements and botanicals (2013), AOAC Int. 1–38. Search in Google Scholar

2. Barison, A., Da Silva, C.W.P., Campos, F.R., Simonelli, F., Lenz, C.A. & Ferreira. A.G. (2010). A simple methodology for the determination of fatty acid composition in edible oils through 1H NMR spectroscopy. Magn. Reson. Chem., 48(8), 642–650. DOI: 10.1002/mrc.2629.20589730 Apri DOISearch in Google Scholar

3. Bartošová, A. & Štefko. T. (2017). Gas Chromatographic Determination of Fatty Acids in Oils with Regard to the Assessment of Fire Hazard. Res. Pap. Fac. Mater. Sci. Technol. Slovak Univ. Technol. 25, 73–81. DOI: 10.1515/rput-2017-0009. Apri DOISearch in Google Scholar

4. Blumhorst, M.R., Venkitasubramanian, P. & Collison, M.W. (2011). Direct determination of glycidyl esters of fatty acids in vegetable Oils by LC-MS. JAOCS. J. Am. Oil Chem. Soc., 88(9), 1275–1283. DOI: 10.1007/s11746-011-1873-1.314332321909156 Apri DOISearch in Google Scholar

5. Carvalho, M.S., Mendonça, M.A., Pinho, D.M.M., Resck, I.S. & Suarez, P.A.Z. (2012). Chromatographic analyses of fatty acid methyl esters by HPLC-UV and GC-FID. J. Braz. Chem. Soc., 23(4), 763–769. DOI: 10.1590/S0103-50532012000400023. Apri DOISearch in Google Scholar

6. Council of Europe (2017). European Pharmacopoeia 9th edition. Search in Google Scholar

7. Freitas, H.R. (2017). Chlorella vulgaris as a Source of Essential Fatty Acids and Micronutrients: A Brief Commentary. The Open Plant Science Journal, 10(1), 92-99. DOI: 10.2174/1874294701710010092. Apri DOISearch in Google Scholar

8. Khoury, S., Canlet, C., Lacroix, M.Z., Berdeaux, O., Jouhet, J. & Bertrand-Michel, J. (2018). Quantification of lipids: Model. reality. and compromise. Biomolecules, 8(4), 174. DOI: 10.3390/biom8040174.631682830558107 Apri DOISearch in Google Scholar

9. Klug, L. & Daum, G. (2014). Yeast lipid metabolism at a glance. FEMS Yeast Res., 14(3), 369–388. DOI: 10.1111/1567-1364.12141.24520995 Apri DOISearch in Google Scholar

10. Marcone, M.F., Wang, S., Albabish, W., Nie, S., Somnarain, D. & Hill. A. (2013). Diverse food-based applications of nuclear magnetic resonance (NMR) technology. Food Res. Int., 51(2), 729–747. DOI: 10.1016/j.foodres.2012.12.046. Apri DOISearch in Google Scholar

11. Martin, C.E., Oh, C.S. & Jiang, Y. (2007). Regulation of long chain unsaturated fatty acid synthesis in yeast. Biochim. Biophys. Acta - Mol. Cell Biol. Lipids, 1771(3), 271–285. DOI: 10.1016/j.bbalip.2006.06.010.16920014 Apri DOISearch in Google Scholar

12. Miranda, A.M., Castilho-Almeida, E.W., Martins Ferreira, E.H., Moreira, G.F., Achete, C.A., Armond, R.A.S.Z., Dos Santos, H.F. & Jorio, A. (2014). Line shape analysis of the Raman spectra from pure and mixed biofuels esters compounds. Fuel, 115, 118–125. DOI: 10.1016/j.fuel.2013.06.038. Apri DOISearch in Google Scholar

13. Nyiri, Z., Novák, M., Bodai, Z., Petrovics, N., Eke, Z. (2017). Determination of polycyclic aromatic hydrocarbons in infant formula using solid state urea clathrate formation with gas chromatography – tandem mass spectrometry. Talanta, 174, 214–220. DOI: 10.1016/j.talanta.2017.05.065.28738571 Apri DOISearch in Google Scholar

14. Petrović, M., Kezić, N. & Bolanča. V. (2010). Optimization of the GC method for routine analysis of the fatty acid profile in several food samples. Food Chem, 122(1), 285–291. DOI: 10.1016/j.foodchem.2010.02.018. Apri DOISearch in Google Scholar

15. Potocki, L., Baran, A., Oklejewicz, B., Szpyrka, E., Podbielska, M. & Schwarzbacherová, V. (2020). Synthetic Pesticides Used in Agricultural Production Promote Genetic Instability and Metabolic Variability in Candida spp. Genes, 11(8), 848. DOI: 10.3390/genes11080848.746377032722318 Apri DOISearch in Google Scholar

16. Ren, J., Mozurkewich, E.; Sen, A., Vahratian, A., Ferreri, T., Morse, A. & Djuric, Z. (2013). Total Serum Fatty Acid Analysis by GC-MS: Assay Validation and Serum Sample Stability. Curr. Pharm. Anal., 9(4), 331–339. DOI: 10.2174/1573412911309040002.412375725110470 Apri DOISearch in Google Scholar

17. Rogóż, J., Podbielska, M., Szpyrka, E. & Wnuk, M. (2021). Characteristics of Dietary Fatty Acids Isolated from Historic Dental Calculus of the 17th- and 18th-Century Inhabitants of the Subcarpathian Region (Poland). Molecules, 26(10), 2951. DOI: 10.3390/molecules26102951.815589134063539 Apri DOISearch in Google Scholar

18. Rousseaux, M.C., Cherbiy-Hoffmann, S.U., Hall, A.J. & Searles, P.S. (2020). Fatty acid composition of olive oil in response to fruit canopy position and artificial shading. Sci. Hortic., 271, 109477. DOI: 10.1016/j.scienta.2020.109477. Apri DOISearch in Google Scholar

19. Schiavon, S., Pellattiero, E., Cecchinato, A., Tagliapietra, F., Dannenberger, D., Nuernberg, K., Nuernberg, G. & Bittante, G. (2016). The influence of different sample preparation procedures on the determination of fatty acid profiles of beef subcutaneous fat. liver and muscle by gas chromatography. J. Food Compos. Anal., 50, 10–18. DOI: 10.1016/j.jfca.2016.05.001. Apri DOISearch in Google Scholar

20. Schwarzinger, B., Feichtinger, M., Blank-Landeshammer, B., Weghuber, J. & Schwarzinger, C. (2022). Quick determination of erucic acid in mustard oils and seeds. Journal of Analytical and Applied Pyrolysis, 164, 105523. DOI: 10.1016/j.jaap.2022.105523. Apri DOISearch in Google Scholar

21. Sherazi, S.T.H., Arain, S., Mahesar, S.A., Bhanger, M.I. & Khaskheli, A.R. (2013). Erucic acid evaluation in rapeseed and canola oil by Fourier transform-infrared spectroscopy. Eur. J. Lipid Sci. Technol., 115(5), 535–540. DOI: 10.1002/ejlt.201200272. Apri DOISearch in Google Scholar

22. Simopoulos, AP. (2008). The importance of the omega-6/omega-3 fatty acid ratio in cardiovascular disease and other chronic diseases. Exp Biol Med (Maywood), 233(6), 674-88. DOI: 10.3181/0711-MR-311.18408140 Apri DOISearch in Google Scholar

23. Słowik-Borowiec, M., Zdeb, G., Kuras, W. & Książek-Trela, P. (2022). Influence of Bacillus subtilis fermentation on content of selected macronutrients in seeds and beans. Acta Universitatis Cibiniensis. Series E: Food Technology, 26(1), 123-138. DOI: 10.2478/aucft-2022-0010. Apri DOISearch in Google Scholar

24. Syed, M.B. (2017). Analysis of biodiesel by high performance liquid chromatography using refractive index detector. MethodsX, 4, 256–259. DOI: 10.1016/j.mex.2017.07.002. Apri DOISearch in Google Scholar

25. Szpyrka, E., Broda, D., Oklejewicz, B., Podbielska, M., Slowik-Borowiec, M., Jagusztyn, B., Chrzanowski, G., Kus-Liskiewicz, M., Duda, M., Zuczek, J., Wnuk, M. & Lewinska, A. (2020). A Non-Vector Approach to Increase Lipid Levels in the Microalga Planktochlorella nurekis. Molecules, 25(2), 270. DOI: 10.3390/molecules25020270. Apri DOISearch in Google Scholar

26. Tuller, G., Nemec, T., Hrastnik, C. & DauM, G. (1999). Lipid composition of subcellular membranes of an FY1679-derived haploid yeast wild-type strain grown on different carbon sources. Yeast, 15(14), 1555–1564. DOI: 10.1002/(SICI)1097-0061(199910)15:14<1555::AID-YEA479>3.0.CO;2-Z. Apri DOISearch in Google Scholar

27. Tyburczy, C., Mossoba, M.M. & Rader, J.I. (2013). Determination of trans fat in edible oils: Current official methods and overview of recent developments Functional Foods and Dietary Supplements. Anal. Bioanal. Chem., 405(17), 5759–5772. DOI: 10.1007/s00216-013-7005-z. Apri DOISearch in Google Scholar

28. Van Wychen, S., Ramirez, K. & Laurens, L.M.L. (2013). Determination of Total Lipids as Fatty Acid Methyl Esters (FAME) by in situ Transesterification. Contract, 303, 275–3000. Search in Google Scholar

29. Wilczynska, A. & Modrzewski, A.F. (2018). Chapter 15 – Fatty acids in human diet and their impact on cognitive and emotional functioning. The Role of Functional Food Security in Global Health., 261–270. DOI: 10.1016/B978-0-12-813148-0.00015-3. Apri DOISearch in Google Scholar

30. Yanty, N.A.M., Marikkar, J.M.N. & Abdulkarim, S.M. (2014). Determination of types of fat ingredient in some commercial biscuit formulations. Int. Food Res. J., 21(1), 277–282. Search in Google Scholar

31. Zhang, Z.S., Wang, S., Liu, H., Li, B.Z. & Che, L. (2020). Constituents and thermal properties of milk thistle seed oils extracted with three methods. LWT, 126, 109282. DOI: 10.1016/j.lwt.2020.109282. Apri DOISearch in Google Scholar

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