Design of Draw Resistance of Pressure Drop Standards for Tobacco Products Based on the Flow Distribution
Published Online: Aug 10, 2024
Page range: 164 - 172
Received: Aug 18, 2023
Accepted: Apr 24, 2024
DOI: https://doi.org/10.2478/cttr-2024-0006
Keywords
© 2024 Pengfei Zhang et al., published by Sciendo
This work is licensed under the Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License.
Cigarette draw resistance and filter pressure drop are both major physical parameters that affect the composition of cigarette smoke and sensory quality (1). The tobacco industry measures draw resistance of cigarettes and filter pressure drop by means of specific testing equipment, which is calibrated with pressure drop transfer standards. The ISO 6565 standard (2) specifies the basic characteristics of the pressure drop standards and calibration methods. Currently, there exist many studies on the calibration method and environmental conditions of the pressure drop standard. The tobacco industry carries out metrological calibration of the pressure drop standard based on ISO 6565. Y
Most of the current research focuses on the calibration method of the pressure drop standard and the effect of environmental conditions on the pressure drop standard, but there are no reports on methods for quantitative calculation of the internal air flow in the pressure drop standard. Based on the structural parameters of a pressure drop standard containing ten parallel capillaries, a flow model was established including the effects of the laminar flow in the inlet section and the flow distribution in the capillaries.
This model allowed calculating the draw resistance of the pressure drop standard, which can provide theoretical guidance for the design of the pressure drop standard.
Seven pressure drop standards with specifications of around 1–8 kPa, numbered 1–7, and conditioned according to ISO 4302 (7) for 48 hours.
Digital pressure gauge Fluke RPM4 (Fluke, Everett, WA, USA); Critical Flow Orifice (CFO) standard (Cerulean, Milton Keynes, UK); Optical gaging products (OGP) vision measurement system (Hexagon, Stockholm, Sweden) with a resolution of 1 μm.
The structural parameters, including capillary diameter and overall length of pressure drop standards were measured using an OGP image measurement device. The pressure drop standard was fixed using a clamping device so that the cross-section of the standard was parallel to the bottom surface of the test bench. OGP's camera focused on the end face of the standard. The experimental instrumentation is shown in Figure 1.

Optical gaging product (OGP) test instrumentarium.
Commencing from a reference point, the diameters of the ten capillaries were measured in clockwise manner and denoted as d1 to d10 successively. The left panel of Figure 2 illustrates a schematic representation of the end face of the pressure drop standard, while the right panel shows a length diagram of the pressure drop standard. The pressure drop standard was placed horizontally on the test stand and the test software was opened. After that, one end of the standard was searched to draw a boundary line. The camera movement was used to find the other end of the rod to perform the same operation. The software was used to determine the distance between the two lines, i.e. the length of the standard. During empirical testing, we observed that the data from both ends of the pressure drop standard exhibited minimal variance. Consequently, we selected the geometric data from one end for documentation in Table 1. Standard constant flow orifice (CFO) calibration of the pressure drop standard is illustrated in Figure 3. The gas flow rate at the output end of the pressure drop standard controlled by the standard constant flow orifice should be 17.50 ± 0.30 mL/s. Initially, the gas supply switch was turned on, all flow resistances were removed to zero the pressure difference gauge, and the digital differential pressure gauge was zeroed. Then, the pressure drop standard was placed in a dedicated fixture, the air valve was opened, and the pressure difference between the two ends of the rod was tested using a digital differential pressure gauge. Recordings were taken at 2-min intervals, capturing data five times until a state of stability was reached, indicated by no further changes in the reading after 10 min. This final reading represented the draw resistance of the pressure drop standard.

Geometric structure and schematic diagram of pressure drop standards.
Geometric parameters of pressure drop standard.
Parameter | Capillary no. (mm) |
|||||||||
---|---|---|---|---|---|---|---|---|---|---|
d1 | d2 | d3 | d4 | d5 | d6 | d7 | d8 | d9 | d10 | |
Inner diameter of capillary | 0.643 | 0.635 | 0.634 | 0.635 | 0.630 | 0.630 | 0.622 | 0.637 | 0.640 | 0.635 |
Diameter of pressure drop standard | 7.981 | |||||||||
Length of pressure drop standard | 120.432 |

Schematic diagram of pressure drop standard calibration device based on the critical flow orifice (CFO) method.
The measurement process was repeated three times, and the average reading obtained at the 10-min mark served as the calibrated value for the pressure drop standard. The calibration results were reported with a precision of 0.1 Pa.
The flow of the gas passing through a capillary of the pressure drop standard can be regarded as laminar flow in a circular capillary. After the gas flows into the capillary at a uniform velocity

Schematic diagram of the developing and fully developed flow sections in a capillary of the pressure drop standard.

Velocity cloud diagrams of the inlet and outlet sections.
The pressure drop along a rough capillary in steady flow of an incompressible viscous fluid is related to the length of the capillary
Let
Equation [2] is applicable to both laminar and turbulent flows. The volumetric flow rate
The total flow resistance
So:
The total flow resistance
According to W
The pressure loss coefficient
As shown in Figure 6, the pressure drop from the inlet section to the i-th section in the developing section, which is divided into

Schematic diagram of segmentation in the developing section.
The relationship between the pressure loss coefficient
Combined with equation [7], the flow resistance of the developing section can be expressed as:
The flow in the developed section is laminar. According to N
Combined with the calculated length
Based on the above analysis, an iterative calculation algorithm was established, as shown in Figure 7. In accordance with the previously mentioned resistance theory, given the pressure drop value, we could verify the value by calculating with the theoretical capillary diameter. To validate the accuracy of the theory, seven pressure drop standards were created. An iterative approach was used to guide the allowable deviation in the theoretical diameter of the pressure drop standards and to instruct the deviation of the pressure drop standards based on the range of diameter variations. Given that the total flow rate was constant and as an initial condition for the iteration, the flow rate was set so that it was equally distributed across the capillaries. However, due to slight differences in the diameter and length of each capillary, after one iteration, the flow rate for each capillary would also differ. Therefore, multiple iterations were carried out to obtain more accurate flow rates for each capillary and ultimately to calculate a more precise value of draw resistance. This algorithm was capable of converging to a precise value, primarily due to its explicit optimization objective: the pressure drops of the pressure drop standards. In each iteration, the algorithm updates the flow rate of each capillary to calculate the pressure drop of the pressure drop standard. Moreover, the algorithm's termination condition was set such that when the difference between the pressure drops in two consecutive iterations was less than 0.001, the algorithm ceased to iterate. This termination condition is a typical criterion for convergence. If this condition is met within a finite number of iterations, we could assert that the algorithm had indeed converged.

The program was designed according to the MVVM (Model-View-View model) pattern. The view was responsible for the appearance of the interface of the entire program, the view model was responsible for modeling the content presented in the interface, and the model was also used to store data. The interface was developed using WPF (Windows Presentation Foundation), the latest generation of Microsoft's graphics system, and the logical functions of the program were implemented in C#.
The program allows for the input of experimental environmental parameters (temperature, humidity, atmospheric pressure) and reads the diameter and length of the ten capillaries of the pressure drop standard obtained from OGP testing in a comma-separated values (CSV) format. Following the logic outlined in theoretical analysis, the program performed iterative calculations.
The iteration process was guided by the criterion that the difference in pressure drop between two consecutive steps should be below 10−3 Pa or reached the maximum number of iterations, upon which the calculation loop was terminated. Ultimately, the program computed the draw resistance of the pressure drop standard, the flow rate for each capillary, and the proportion of the development length to the total length. The results were then displayed in the interface, providing a comprehensive presentation of the calculations performed.
Experimental testing was conducted on seven different specifications of pressure drop standards using an optical gaging product (OGP). This led to the acquisition of geometric structure data for the draw resistance standard rods. The results are presented in Table 2.
Inner diameter parameter table of different pressure drop standards.
Sample ID | Capillary no. (mm) |
|||||||||
---|---|---|---|---|---|---|---|---|---|---|
d1 | d2 | d3 | d4 | d5 | d6 | d7 | d8 | d9 | d10 | |
1 | 0.643 | 0.635 | 0.634 | 0.635 | 0.630 | 0.630 | 0.622 | 0.637 | 0.640 | 0.635 |
2 | 0.538 | 0.532 | 0.543 | 0.539 | 0.545 | 0.548 | 0.544 | 0.548 | 0.536 | 0.542 |
3 | 0.479 | 0.484 | 0.485 | 0.477 | 0.491 | 0.486 | 0.481 | 0.484 | 0.478 | 0.480 |
4 | 0.452 | 0.442 | 0.480 | 0.463 | 0.454 | 0.458 | 0.450 | 0.463 | 0.445 | 0.452 |
5 | 0.432 | 0.417 | 0.429 | 0.422 | 0.418 | 0.417 | 0.427 | 0.416 | 0.413 | 0.424 |
6 | 0.413 | 0.422 | 0.412 | 0.415 | 0.432 | 0.428 | 0.420 | 0.418 | 0.414 | 0.427 |
7 | 0.372 | 0.376 | 0.376 | 0.378 | 0.380 | 0.389 | 0.374 | 0.376 | 0.400 | 0.384 |
The theoretical pressure drop values under the corresponding environmental conditions were obtained by iterative calculations of the program, and the comparison results are shown in Table 3.
Comparison of experimental and calculated values.
Sample ID | Experimental draw resistance (Pa) | Calculated draw resistance (Pa) | Relative error (%) |
---|---|---|---|
1 | 980.6 | 974.39 | −0.63 |
2 | 1972.0 | 1875.04 | −7.10 |
3 | 2916.2 | 2903.03 | −0.45 |
4 | 3805.2 | 3634.33 | −4.49 |
5 | 4825.1 | 4836.75 | 0.24 |
6 | 5712.2 | 5377.19 | −5.86 |
7 | 7971.9 | 7513.70 | −5.75 |
The data presented in Table 3 demonstrate a consistent trend between the experimental and calculated values, with all relative errors falling below 8%. This consistency underscores the reliability of our methods and calculations. However, it is important to note that the pressure drop standard, due to its manufacturing process, does not always exhibit a perfect circular shape in its capillaries. This imperfection is a contributing factor to the observed errors. Despite this, the overall trend remains consistent, reinforcing the validity of our approach. A comparative analysis of the experimental and calculated values is illustrated in Figure 8. This visual representation further elucidates the correlation between these two sets of data, providing a clear and comprehensive overview of our findings.

Comparison of experimental and calculated values.
In the area of commercially available pressure drop standards, the prevailing practice relies on empirical methods for designing the dimensions of the capillaries, followed by their one-time encapsulation using capillary glass tubes and epoxy or acrylic resin. However, this design approach lacks a sound theoretical basis, leading to a relatively low qualification rate of the pressure drop standards. To address this issue, we undertook a research study focusing on pressure drop standards with varying structural parameters, and developed a mathematical model to investigate the internal airflow dynamics within these standards. The mathematical model took into account the distribution characteristics of the internal airflow within the pressure drop standards, encompassing laminar inlet effects and the development and fully developed zones inside the capillary. These factors have the potential to impact the suction resistance values of the pressure drop standards. Existing models, in contrast, may overlook these factors, relying solely on energy loss coefficients to characterize the flow dynamics of pressure drop standards. Consequently, the mathematical model was poised to more accurately depict the internal airflow state of the pressure drop standards, thereby enhancing predictive capabilities. Utilizing this model, we calculated the relationship between the dimensions (diameter and length) of the capillaries in the pressure drop standard and the corresponding flow rate and draw resistance. In order to validate our model, we compared experimentally measured draw resistance values of the pressure drop standards with their corresponding theoretical values. Based on the results presented in Table 3, we observed that, for the seven different pressure drop standards, the model yielded a prediction error that was generally below 8%. These findings provide a solid theoretical foundation for the design and manufacturing of pressure drop standards, thus contributing to their overall improvement.
In this paper, the diameter and length of the capillaries in a pressure drop standard were measured by OGP image measuring instrument, and a theoretical model of the gas flow in the pressure drop standard was established based on the flow distribution according to the theory of laminar flow in circular tubes including a turbulent inlet section, and an iterative calculation program was written. The theoretical and experimental differential pressure values of seven pressure drop standards were compared and analyzed. The trends of the theoretical and experimental values did not show significant differences, and the relative errors were below 8%, so the theoretical model can provide support for the design of pressure drop standards.