Volume 40 (2013): Issue 4 (December 2013) Special Issue Title: Proceedings of the 3rd Asia Pacific Conference on Luminescence and Electron Spin Resonance Dating Okayama, Japan, 2012
Volume 40 (2013): Issue 3 (September 2013)
Volume 40 (2013): Issue 2 (June 2013)
Volume 40 (2013): Issue 1 (March 2013)
Volume 39 (2012): Issue 4 (December 2012)
Volume 39 (2012): Issue 3 (September 2012)
Volume 39 (2012): Issue 2 (June 2012)
Volume 39 (2012): Issue 1 (March 2012)
Volume 38 (2011): Issue 4 (December 2011)
Volume 38 (2011): Issue 3 (September 2011) Special Issue Title: Proceedings of the 2nd Asia Pacific Conference on Luminescence Dating, Ahmedabad, India, 2009. Part II Issue Editors: Andrzej Bluszcz, Silesian University of Technology, Gliwice, Poland. Andrzej.Bluszcz@polsl.pl Sheng-Hua Li, The University of Hong Kong, Hong Kong, China. shli@hku.hk Ashok Kumar Singhvi, Physical Research Laboratory, Ahmedabad, India. singhvi@prl.res.in
Volume 38 (2011): Issue 2 (June 2011)
Volume 38 (2011): Issue 1 (March 2011)
Volume 37 (2010): Issue -1 (December 2010) Proceedings of the 2 Asia Pacific Conference on Luminescence Dating, Ahmedabad, India, 2009. Part I
Editors Andrzej Bluszcz, Sheng-Hua Li and Ashok Kumar Singhvi
Published Online: 16 Mar 2013 Page range: 90 - 100
Abstract
Abstract
This paper develops a simplified Bayesian approach to evaluate a luminescence age. We limit our purpose to the cause-effect relationship between the age and the accumulated dose. The accumulated dose is given as a function of the age and several others parameters: internal radionuclides contents, gamma dose rate, cosmic dose rate, alpha efficiency, wetness, conversion factors, wetness coefficients, fading rate and storage time. The age is the quantity we are looking for. Bayes’ theorem expresses the changes on the probability distribution of age due to the luminescence study. The information before study (prior) comprises what is previously known about the age and the archaeological model (cultural period, stratigraphic relations, type, etc.) as well as the parameters of the physical model. The accumulated dose consists in the data describing the measurement. The various stages of Bayesian approach were implemented using the software WinBugs. Simulated data sets were used in various models. We present various small models representing typical examples encountered in luminescence dating.
Published Online: 16 Mar 2013 Page range: 101 - 112
Abstract
Abstract
It has been suggested that the standardized growth curve (SGC) method can be used to accurately determinate equivalent dose (De) and reduce measurement time. However, different opinions regarding the applicability of the SGC method exist. In this paper, we evaluated quartz OSL SGCs of marine and coastal sediments of different grain sizes and different cores in the south Bohai Sea in China, and tested their applicability to the determination of De values. Our results suggested as follows: (1) The SGC method is applicable to both multiple- and single-aliquot regenerative-dose (MAR and SAR) protocols of OSL dating and efficiently provides reliable estimates of De. (2) Finesand quartz of different palaeodoses showed highly similar dose-response curves and an SGC was developed, but old samples using the SGC method have large uncertainties. (3) For coarse-silt quartz, two different types of dose-response curves were recorded: low-dose (≤60Gy) and high-dose (≥100Gy). The growth curves of low-dose quartz were similar to each other, facilitating the use of SGC in De estimations, but errors tended to be larger than those obtained in the SAR method. For high-dose (100–300Gy) quartz, the SGC was also found to be reliable, but there was large uncertainty in De (>300Gy) estimation. We suggest that SGC could be employed for the dating of marine and coastal sediments dating using either MAR or SAR OSL protocol and either fine-silt, coarse-silt or fine-sand quartz.
Published Online: 16 Mar 2013 Page range: 113 - 125
Abstract
Abstract
The absolute chronology of Late Bronze and Early Iron Ages in Polish territories is a result of long-term and complex research. Here, we have investigated the absolute dating of two sites, namely Kłyżów, a cemetery of the Tarnobrzeg Lusatian culture, and Jarosław, a settlement spanning from the late phase of the former to Pomeranian culture, possibly with Jastorf elements. Having been spurred by promising results of thermoluminescence (TL) dating of medieval and Przeworsk materials, we have employed it in those situations, where no other chronometric methods seem to be efficient. TL dating has been combined with typological analysis of the dated pottery and, partially, with radiocarbon method. Albeit the produced TL dates do not represent the level of sought-for fine chronological resolution, they indicate the temporal trends and corroborate the typological research. Our study has shown the potential of TL dating for periods with plateaus on 14C calibration curve. We also have dealt with unexpected TL ages and suggested some solutions of the problem. Finally, we have demonstrated that the condition sine qua non for archaeological interpretation of TL dates is a thorough stylistic-chronological analysis of dated pottery and clear understanding of relations between chronometric dates and the archaeological event to be dated.
Published Online: 16 Mar 2013 Page range: 126 - 133
Abstract
Abstract
Investigations of soil erosion by 137Cs method brings uncertainties of different nature. The estimation of the 137Cs local inventory is associated with problems of data comparison and instrumental errors. In order to avoid systematic errors, the rate of soil erosion determined by the 137Cs method is compared with the values obtained for other radioactive elements. Soil parameters must be regarded too. The aim of the work was to test the character of 137Cs and 40K distribution in the topsoil vertical section for determination erosion-accumulation type and ratio in different time spans. The topsoil thickened by different types of erosion-accumulation processes was sampled at a 2–3 cm interval. Soil samples were analysed by means of scintillation gamma spectrometry. The relationship between 137Cs and 40K inventories was weakest in the topsoil formed by mixing of soil material during the installation of artificial drains. Based on climatic characteristics, variations of theoretical soil accumulation rate in the last 50 years were calculated for the topsoil accumulated predominantly by water erosion. 40K and 137Cs correlation in the bottom of vertical section of topsoil or arable horizon are closest and this section may be used as a complementary parameter determining the local inventory value.
Published Online: 16 Mar 2013 Page range: 134 - 144
Abstract
Abstract
Detailed cathodoluminescence (CL) imaging of zircon crystals, coupled with Laser Ablation Multi-Collector Inductively Coupled Plasma Mass Spectrometry (LA-MC-ICP-MS) U-Pb zircon dating was used to develop new insights into the evolution of granitoids from the High Tatra Mountains. The zircon U-Pb results show two distinct age groups (350±5 Ma and 337±6 Ma) recorded from cores and rims domains, respectively. Obtained results point that the last magmatic activity in the Tatra granitoid intrusion occurred at ca. 330 Ma. The previously suggested age of 314 Ma reflects rather the hydrothermal activity and Pb-loss, coupled with post-magmatic shearing.
Published Online: 16 Mar 2013 Page range: 145 - 152
Abstract
Abstract
We present the first analysis of the influence of climate change on carbon and oxygen isotope fractionation factors for two saccharides (glucose and α-cellulose) of pine wood. The conifers grew in the Niepołomice Forest in Poland and the annual rings covered a time span from 1935 to 2000 AD. Glucose samples from acid hydrolysis of α-cellulose were extracted from annual tree rings. The carbon and oxygen isotope fractionation factors between glucose and α-cellulose were not stable over time. The mean value for the carbon isotope fractionation factors between glucose and α-cellulose was greater than unity. The mean value for the oxygen isotope fractionation factors between glucose and α-cellulose was lower than unity. We established, with respect to climate change, the significance of the interannual and intraannual variation in the carbon and oxygen isotope fractionation factors between both saccharides. We used moving interval correlation results for May of the previous year through September of the current year using a base length of 48 years. The relationship with summer temperature is the main climate signal in the carbon isotope fractionation factor between glucose and α-cellulose. The relationship with autumn sunshine is the main climate signal in the oxygen isotope fractionation factor between glucose and α-cellulose for the tree ring chronology.
This paper develops a simplified Bayesian approach to evaluate a luminescence age. We limit our purpose to the cause-effect relationship between the age and the accumulated dose. The accumulated dose is given as a function of the age and several others parameters: internal radionuclides contents, gamma dose rate, cosmic dose rate, alpha efficiency, wetness, conversion factors, wetness coefficients, fading rate and storage time. The age is the quantity we are looking for. Bayes’ theorem expresses the changes on the probability distribution of age due to the luminescence study. The information before study (prior) comprises what is previously known about the age and the archaeological model (cultural period, stratigraphic relations, type, etc.) as well as the parameters of the physical model. The accumulated dose consists in the data describing the measurement. The various stages of Bayesian approach were implemented using the software WinBugs. Simulated data sets were used in various models. We present various small models representing typical examples encountered in luminescence dating.
It has been suggested that the standardized growth curve (SGC) method can be used to accurately determinate equivalent dose (De) and reduce measurement time. However, different opinions regarding the applicability of the SGC method exist. In this paper, we evaluated quartz OSL SGCs of marine and coastal sediments of different grain sizes and different cores in the south Bohai Sea in China, and tested their applicability to the determination of De values. Our results suggested as follows: (1) The SGC method is applicable to both multiple- and single-aliquot regenerative-dose (MAR and SAR) protocols of OSL dating and efficiently provides reliable estimates of De. (2) Finesand quartz of different palaeodoses showed highly similar dose-response curves and an SGC was developed, but old samples using the SGC method have large uncertainties. (3) For coarse-silt quartz, two different types of dose-response curves were recorded: low-dose (≤60Gy) and high-dose (≥100Gy). The growth curves of low-dose quartz were similar to each other, facilitating the use of SGC in De estimations, but errors tended to be larger than those obtained in the SAR method. For high-dose (100–300Gy) quartz, the SGC was also found to be reliable, but there was large uncertainty in De (>300Gy) estimation. We suggest that SGC could be employed for the dating of marine and coastal sediments dating using either MAR or SAR OSL protocol and either fine-silt, coarse-silt or fine-sand quartz.
The absolute chronology of Late Bronze and Early Iron Ages in Polish territories is a result of long-term and complex research. Here, we have investigated the absolute dating of two sites, namely Kłyżów, a cemetery of the Tarnobrzeg Lusatian culture, and Jarosław, a settlement spanning from the late phase of the former to Pomeranian culture, possibly with Jastorf elements. Having been spurred by promising results of thermoluminescence (TL) dating of medieval and Przeworsk materials, we have employed it in those situations, where no other chronometric methods seem to be efficient. TL dating has been combined with typological analysis of the dated pottery and, partially, with radiocarbon method. Albeit the produced TL dates do not represent the level of sought-for fine chronological resolution, they indicate the temporal trends and corroborate the typological research. Our study has shown the potential of TL dating for periods with plateaus on 14C calibration curve. We also have dealt with unexpected TL ages and suggested some solutions of the problem. Finally, we have demonstrated that the condition sine qua non for archaeological interpretation of TL dates is a thorough stylistic-chronological analysis of dated pottery and clear understanding of relations between chronometric dates and the archaeological event to be dated.
Investigations of soil erosion by 137Cs method brings uncertainties of different nature. The estimation of the 137Cs local inventory is associated with problems of data comparison and instrumental errors. In order to avoid systematic errors, the rate of soil erosion determined by the 137Cs method is compared with the values obtained for other radioactive elements. Soil parameters must be regarded too. The aim of the work was to test the character of 137Cs and 40K distribution in the topsoil vertical section for determination erosion-accumulation type and ratio in different time spans. The topsoil thickened by different types of erosion-accumulation processes was sampled at a 2–3 cm interval. Soil samples were analysed by means of scintillation gamma spectrometry. The relationship between 137Cs and 40K inventories was weakest in the topsoil formed by mixing of soil material during the installation of artificial drains. Based on climatic characteristics, variations of theoretical soil accumulation rate in the last 50 years were calculated for the topsoil accumulated predominantly by water erosion. 40K and 137Cs correlation in the bottom of vertical section of topsoil or arable horizon are closest and this section may be used as a complementary parameter determining the local inventory value.
Detailed cathodoluminescence (CL) imaging of zircon crystals, coupled with Laser Ablation Multi-Collector Inductively Coupled Plasma Mass Spectrometry (LA-MC-ICP-MS) U-Pb zircon dating was used to develop new insights into the evolution of granitoids from the High Tatra Mountains. The zircon U-Pb results show two distinct age groups (350±5 Ma and 337±6 Ma) recorded from cores and rims domains, respectively. Obtained results point that the last magmatic activity in the Tatra granitoid intrusion occurred at ca. 330 Ma. The previously suggested age of 314 Ma reflects rather the hydrothermal activity and Pb-loss, coupled with post-magmatic shearing.
We present the first analysis of the influence of climate change on carbon and oxygen isotope fractionation factors for two saccharides (glucose and α-cellulose) of pine wood. The conifers grew in the Niepołomice Forest in Poland and the annual rings covered a time span from 1935 to 2000 AD. Glucose samples from acid hydrolysis of α-cellulose were extracted from annual tree rings. The carbon and oxygen isotope fractionation factors between glucose and α-cellulose were not stable over time. The mean value for the carbon isotope fractionation factors between glucose and α-cellulose was greater than unity. The mean value for the oxygen isotope fractionation factors between glucose and α-cellulose was lower than unity. We established, with respect to climate change, the significance of the interannual and intraannual variation in the carbon and oxygen isotope fractionation factors between both saccharides. We used moving interval correlation results for May of the previous year through September of the current year using a base length of 48 years. The relationship with summer temperature is the main climate signal in the carbon isotope fractionation factor between glucose and α-cellulose. The relationship with autumn sunshine is the main climate signal in the oxygen isotope fractionation factor between glucose and α-cellulose for the tree ring chronology.