The Application of a Cadmium Reducer and a Diazotisation Reaction for the Determination of Nitrate and Nitrite in Tobacco / Über die Anwendung des Cadmium-Reduktors und der Diazotierung zur Bestimmung von Nitrat und Nitrit im Tabak
13 cze 2014
O artykule
Data publikacji: 13 cze 2014
Zakres stron: 95 - 100
DOI: https://doi.org/10.2478/cttr-2013-0102
Słowa kluczowe
© Beiträge zur Tabakforschung International
This article is distributed under the terms of the Creative Commons Attribution Non-Commercial License, which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.
Nitrate is reduced by means of a cadmium reducer and spectrophotometrically determined in the form of nitrite by a diazotisation reaction. The results obtained by application of the described method to tobacco extracts correspond well to those resulting from the earlier described dimethylphenol procedure. Owing to its better sensitivity and specifity the reduction method is particularly suitable for the quantitative analysis of smallest amounts of nitrate. Quantities of 0.03 % of nitrate can be determined without difficulties. The inferior limit of detection is 0.001 %.