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Synthesis and characterization of CdS nanorods by combined sonochemical-solvothermal method

Pinar Acar Bozkurt

Pinar Acar Bozkurt

Department of Chemistry, Science Faculty, Ankara UniversityAnkara, Turkey
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Bozkurt, Pinar Acar
 e 
Burak Derkuş

Burak Derkuş

Department of Chemistry, Science Faculty, Ankara UniversityAnkara, Turkey
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Derkuş, Burak
  
28 set 2016
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Categoria dell'articolo: Research Article
Pubblicato online: 28 set 2016
Pagine: 684 - 690
Ricevuto: 04 apr 2016
Accettato: 11 lug 2016
DOI: https://doi.org/10.1515/msp-2016-0089
Parole chiave
© 2016 Pinar Acar Bozkurt et al., published by Sciendo
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.

Fig. 1

XRD patterns of CdS nanoparticles synthesized by different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).
XRD patterns of CdS nanoparticles synthesized by different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 2

TEM images of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).
TEM images of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 3

EDX spectrum of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).
EDX spectrum of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 4

Schematic presentation and structural development of synthesized CdS nanoparticles obtained using different experimental procedures.
Schematic presentation and structural development of synthesized CdS nanoparticles obtained using different experimental procedures.

Effects of the experimental conditions on the structure of the CdS nanoparticles_

SampleKind of methodCompositionReaction timeStructure
S1sonochemicalCd(NO3)2 + TAA (1:2)40 mincubic
S2sonochemicalCd(NO3)2 + Na2S (1:2)40 mincubic
S3combined sonochemical-solvothermalCd(NO3)2+ TAA (1:2)40 minhexagonal (irregular)
S4combined sonochemical-solvothermalCd(NO3)2+ TAA (1:4)1 hhexagonal (irregular)
S5combined sonochemical-solvothermalCd(NO3 )2 + Na2S(1:4)1 hhexagonal (irregular)
S6combined sonochemical-solvothermalCd(NO3)2 + Na2S (1:4)5 hhexagonal
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Argomenti della rivista:
Scienze materiali, Scienze materiali, altro, Nanomateriali, Materiali funzionali ed intelligenti, Caratteristica e proprietà dei materiali
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