Accès libre

Synthesis and characterization of CdS nanorods by combined sonochemical-solvothermal method

Pinar Acar Bozkurt

Pinar Acar Bozkurt

Department of Chemistry, Science Faculty, Ankara UniversityAnkara, Turkey
Recherchez cet auteur sur
Sciendo|Google Scholar
Bozkurt, Pinar Acar
 et 
Burak Derkuş

Burak Derkuş

Department of Chemistry, Science Faculty, Ankara UniversityAnkara, Turkey
Recherchez cet auteur sur
Sciendo|Google Scholar
Derkuş, Burak
  
28 sept. 2016
Synthesis and characterization of CdS nanorods by combined sonochemical-solvothermal method's Cover Image
À propos de cet article
Article précédent
Article suivant
Citez
Télécharger la couverture
Catégorie d'article: Research Article
Publié en ligne: 28 sept. 2016
Pages: 684 - 690
Reçu: 04 avr. 2016
Accepté: 11 juil. 2016
DOI: https://doi.org/10.1515/msp-2016-0089
Mots clés
© 2016 Pinar Acar Bozkurt et al., published by Sciendo
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.

Fig. 1

XRD patterns of CdS nanoparticles synthesized by different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).
XRD patterns of CdS nanoparticles synthesized by different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 2

TEM images of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).
TEM images of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 3

EDX spectrum of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).
EDX spectrum of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 4

Schematic presentation and structural development of synthesized CdS nanoparticles obtained using different experimental procedures.
Schematic presentation and structural development of synthesized CdS nanoparticles obtained using different experimental procedures.

Effects of the experimental conditions on the structure of the CdS nanoparticles_

SampleKind of methodCompositionReaction timeStructure
S1sonochemicalCd(NO3)2 + TAA (1:2)40 mincubic
S2sonochemicalCd(NO3)2 + Na2S (1:2)40 mincubic
S3combined sonochemical-solvothermalCd(NO3)2+ TAA (1:2)40 minhexagonal (irregular)
S4combined sonochemical-solvothermalCd(NO3)2+ TAA (1:4)1 hhexagonal (irregular)
S5combined sonochemical-solvothermalCd(NO3 )2 + Na2S(1:4)1 hhexagonal (irregular)
S6combined sonochemical-solvothermalCd(NO3)2 + Na2S (1:4)5 hhexagonal
Langue:
Anglais
Périodicité:
4 fois par an
Sujets de la revue:
Sciences des matériaux, Sciences des matériaux, autres, Nanomatériaux, Matériaux fonctionnels et intelligents, Caractérisation et propriétés des matériaux
RSS Feed de la revue