With reference to a simultaneous determination of hexane-soluble organophosphoric phytopharmaceuticals in vegetables (1), a method for quantitatively analysing residues of chlorfenvinphos, fenitrothion, fenchlorphos, dimephenthoate, chlorpyriphos, parathion-methyl, parathion, phorate, phosvel, phosalone, ethoprophos, methidathion, salithion and tetrachlorvinphos in tobacco has been developed. Recoveries are between 75 % and 124 %, the detection Iimits between 0.01 ppm and 0.1 ppm.