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Insights into the multistep transformation of titanate nanotubes into nanowires and nanoribbons

Agnieszka Baszczuk

Agnieszka Baszczuk

Poland
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Baszczuk, Agnieszka
, 
Marek Jasiorski

Marek Jasiorski

Poland
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Jasiorski, Marek
, 
Beata Borak

Beata Borak

Poland
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Borak, Beata
 and 
Jerzy Wódka

Jerzy Wódka

Poland
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Wódka, Jerzy
  
Nov 17, 2016
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Published Online: Nov 17, 2016
Page range: 691 - 702
Received: Aug 20, 2015
Accepted: Jul 26, 2016
DOI: https://doi.org/10.1515/msp-2016-0094
Keywords
© Wroclaw University of Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.
TEM images of hydrothermal products synthesized at 120 °C for: (A) 24 h, (B) 72 h and (C) 120 h.
TEM images of hydrothermal products synthesized at 120 °C for: (A) 24 h, (B) 72 h and (C) 120 h.
TEM images of hydrothermal products synthesized at 150 °C for: (A) 24 h and (B) 48 h.
TEM images of hydrothermal products synthesized at 150 °C for: (A) 24 h and (B) 48 h.
Electron microscopy images (TEM and SEM) of hydrothermal products synthesized at 200 °C for: (A) 10 h and (B) 24 h.
Electron microscopy images (TEM and SEM) of hydrothermal products synthesized at 200 °C for: (A) 10 h and (B) 24 h.
XRD patterns of materials obtained after hydrothermal synthesis at 120 °C: (b) 24 h, (c) 72 h, (d) 120 h. The XRD pattern of TiO2 raw powder is given in (a) as reference.
XRD patterns of materials obtained after hydrothermal synthesis at 120 °C: (b) 24 h, (c) 72 h, (d) 120 h. The XRD pattern of TiO2 raw powder is given in (a) as reference.
Raman spectra of materials obtained after hydrothermal synthesis at 120 °C: (a) 24 h, (b) 72 h, (c) 120 h.
Raman spectra of materials obtained after hydrothermal synthesis at 120 °C: (a) 24 h, (b) 72 h, (c) 120 h.
Comparison between the XRD patterns of the materials synthesized at 120 °C and 150 °C: (a) 120 °C, 120 h, (b) 150 °C, 24 h and (c) 150 °C 48 h.
Comparison between the XRD patterns of the materials synthesized at 120 °C and 150 °C: (a) 120 °C, 120 h, (b) 150 °C, 24 h and (c) 150 °C 48 h.
Raman spectra of materials obtained after hydrothermal synthesis at 150 °C: (b) 24 h, (c) 48 h and as a reference Raman spectrum of material synthesized at 120 °C for 120 h (a).
Raman spectra of materials obtained after hydrothermal synthesis at 150 °C: (b) 24 h, (c) 48 h and as a reference Raman spectrum of material synthesized at 120 °C for 120 h (a).
XRD patterns of materials after hydrothermal synthesis at 200 °C: (b) 10 h, (c) 24 h and material after hydrothermal synthesis at 150 °C for 72 h (a). The XRD pattern of H2Ti3O7 generated using the data deposited in ICSD database by Gateshki et. al. [18] is given in (d) as reference.
XRD patterns of materials after hydrothermal synthesis at 200 °C: (b) 10 h, (c) 24 h and material after hydrothermal synthesis at 150 °C for 72 h (a). The XRD pattern of H2Ti3O7 generated using the data deposited in ICSD database by Gateshki et. al. [18] is given in (d) as reference.
Raman spectra of materials obtained after hydrothermal synthesis at 200 °C: (b) for 24 h, (c) for 10 h and as a reference Raman spectrum of material synthesized at 150 °C for 48 h (a).
Raman spectra of materials obtained after hydrothermal synthesis at 200 °C: (b) for 24 h, (c) for 10 h and as a reference Raman spectrum of material synthesized at 150 °C for 48 h (a).
Language:
English
Publication timeframe:
4 times per year
Journal Subjects:
Materials Sciences, Materials Sciences, other, Nanomaterials, Functional and Smart Materials, Materials Characterization and Properties
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