The presented work focuses on the influence of the micromaterials (microspheres, aerogel and polymer hydroxyethyl methyl cellulose) on thermal properties of gypsum. The polymer and the aerogel are used as additives in the weight fraction, up to 1% of pure gypsum and the microspheres in the weight fraction, up to 10% of gypsum. The water-to-gypsum ratio was at the level of 0.75. Non-stationary method and Isomet 2114 experimental setup were applied for the purpose of measurements of thermal parameters. The coefficient of thermal conductivity