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Effect of silane coating surface treatment on friction and wear properties of carbon fiber/PI composites

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Fig. 1

The schematic diagram of the friction pair.
The schematic diagram of the friction pair.

Fig. 2

Scanning electron micrograph of CF (a: untreated, b: 1wt% silane coating, c: 2wt% silane coating, and d: 3wt% silane coating).
Scanning electron micrograph of CF (a: untreated, b: 1wt% silane coating, c: 2wt% silane coating, and d: 3wt% silane coating).

Fig. 3

Cross-sectional scanning electron micrographs of CF/PI (a: untreated, b: 1wt% silane coating, c: 2wt% silane coating, and d: 3wt% silane coating).
Cross-sectional scanning electron micrographs of CF/PI (a: untreated, b: 1wt% silane coating, c: 2wt% silane coating, and d: 3wt% silane coating).

Fig. 4

The tensile strength of the composites (a: untreated, b: 1wt% silane coating, c: 2wt% silane coating, and d: 3wt% silane coating).
The tensile strength of the composites (a: untreated, b: 1wt% silane coating, c: 2wt% silane coating, and d: 3wt% silane coating).

Fig. 5

SEM photographs of the composite after wear (a: untreated, b: 1wt% silane coating, c: 2wt% silane coating, and d: 3wt% silane coating).
SEM photographs of the composite after wear (a: untreated, b: 1wt% silane coating, c: 2wt% silane coating, and d: 3wt% silane coating).

Fig. 6

The coefficient of friction and wear rate of the composite (a: untreated, b: 1wt% silane coating, c: 2wt% silane coating, and d: 3wt% silane coating).
The coefficient of friction and wear rate of the composite (a: untreated, b: 1wt% silane coating, c: 2wt% silane coating, and d: 3wt% silane coating).

Fig. 7

SEM micrographs of transfer film on the coupling surface (a: untreated and b: 3wt% silane coating).
SEM micrographs of transfer film on the coupling surface (a: untreated and b: 3wt% silane coating).

Surface elementary composition of carbon fibers.

Surface treatment Elementary composition / % Atom ratio / %

C O N Si2p O/C N/C

Untreated 82.3 10.2 7.5 12.4 8.9
0.1% coating 77.7 13.1 8.4 0.8 16.9 10.7
0.2% coating 75.3 14.4 9.1 1.2 19.1 12.1
0.3% coating 76.9 13.2 8.47 1.42 17.2 11.0

Main properties of PI (GCTPTM).

Density (kg/m3) 1350 Impact strength (kJ/m2) 25
Tensile Strength (MPa) 95 Thermal expansion coefficient (°C−1) 4.8 × 10−5
Elongation at break (%) 7 Tg (°C) 260
Flexural strength (MPa) 150 Thermal decomposition temperature (°C) 240

Chemical composition of GCr15 steel (wt %).

C Si Mn Cr P S Fe
0.95–1.05 0.15–0.35 0.2–0.4 1.30–1.65 ⩽ 0.027 ⩽ 0.02 Remainder
eISSN:
2083-134X
Langue:
Anglais