Synthesis of a novel UV-curable prepolymer 1,3-bis[(3-ethyl-3-methoxyoxetane)propyl]tetramethyldisiloxane and study on its UV-curing properties

[1] Decker C. Kinetic study and new applications of UV radiation curing. Macromol Rapid Commun. 2003;23(18):1067–93. https://doi.org/10.1002/marc.200290014. DeckerC Kinetic study and new applications of UV radiation curing Macromol Rapid Commun 2003 23 18 1067 93 https://doi.org/10.1002/marc.200290014. 10.1002/marc.200290014 Search in Google Scholar

[2] Shirai M. Reworkable UV curing materials. Prog Organic Coat. 2007;58(2–3):158–65. https://doi.org/10.1016/j.porgcoat.2006.08.022. ShiraiM Reworkable UV curing materials Prog Organic Coat 2007 58 2–3 158 65 https://doi.org/10.1016/j.porgcoat.2006.08.022. 10.1016/j.porgcoat.2006.08.022 Search in Google Scholar

[3] Xie P, Hu L, He J, Kang W, Yang W. Mechanism and solutions of appearance defects on microfluidic chips manufactured by UV-curing assisted injection molding. J Polym Eng. 2017;37(5):493–503. https://doi.org/10.1515/polyeng-2016-0153. XieP HuL HeJ KangW YangW Mechanism and solutions of appearance defects on microfluidic chips manufactured by UV-curing assisted injection molding J Polym Eng 2017 37 5 493 503 https://doi.org/10.1515/polyeng-2016-0153. 10.1515/polyeng-2016-0153 Search in Google Scholar

[4] Sangermano M, Razza N, Crivello JV. Cationic UV-curing: Technology and applications. Macromol Mater Eng. 2014;299(7):775–93. https://doi.org/10.1002/mame.201300349. SangermanoM RazzaN CrivelloJV Cationic UV-curing: Technology and applications Macromol Mater Eng 2014 299 7 775 93 https://doi.org/10.1002/mame.201300349. 10.1002/mame.201300349 Search in Google Scholar

[5] Kraft V, Schumann C, Salzmann D, Nopper H, Weyhe D, Schenk A. Towards realistic organ models for 3D printing and visualization. Curr Dir Biomed Eng. 2021;7(1):166–70. https://doi.org/10.1515/cdbme-2021-1036. KraftV SchumannC SalzmannD NopperH WeyheD SchenkA Towards realistic organ models for 3D printing and visualization Curr Dir Biomed Eng 2021 7 1 166 70 https://doi.org/10.1515/cdbme-2021-1036. 10.1515/cdbme-2021-1036 Search in Google Scholar

[6] Stansbury JW, Idacavage MJ. 3D printing with polymers: challenges among expanding options and opportunities. Den Mater. 2016;32(1):54–64. https://doi.org/10.1016/j.dental.2015.09.018. StansburyJW IdacavageMJ 3D printing with polymers: challenges among expanding options and opportunities Den Mater 2016 32 1 54 64 https://doi.org/10.1016/j.dental.2015.09.018. 10.1016/j.dental.2015.09.01826494268 Search in Google Scholar

[7] Zhang LJ, Wu CB, Yang F, Geng XY, Li MQ, Xiao JJ. Preparation and characterization of UV curable hybrid system based on free radical and cationic mechanism. Appl Mech Mater. 2014;470:141–45. https://doi.org/10.4028/www.scientific.net/AMM.470.141. ZhangLJ WuCB YangF GengXY LiMQ XiaoJJ Preparation and characterization of UV curable hybrid system based on free radical and cationic mechanism Appl Mech Mater 2014 470 141 45 https://doi.org/10.4028/www.scientific.net/AMM.470.141. 10.4028/www.scientific.net/AMM.470.141 Search in Google Scholar

[8] Park YJ, Lim DH, Kim HJ, Park DS, Sung IK. UV and thermal-curing behaviors of dual-curable adhesives based on epoxy acrylate oligomers. Int J Adhes Adhesives. 2012;29(7):710–7. https://doi.org/10.1016/j.ijadhadh.2009.02.001. ParkYJ LimDH KimHJ ParkDS SungIK UV and thermal-curing behaviors of dual-curable adhesives based on epoxy acrylate oligomers Int J Adhes Adhesives 2012 29 7 710 7 https://doi.org/10.1016/j.ijadhadh.2009.02.001. 10.1016/j.ijadhadh.2009.02.001 Search in Google Scholar

[9] Cho JD, Ju HT, Hong JW. Photocuring kinetics of UV-initiated free-radical photopolymerizations with and without silica nanoparticles. J Polym Sci Part A. 2010;43(3):658–70. https://doi.org/10.1002/pola.20529. ChoJD JuHT HongJW Photocuring kinetics of UV-initiated free-radical photopolymerizations with and without silica nanoparticles J Polym Sci Part A 2010 43 3 658 70 https://doi.org/10.1002/pola.20529. 10.1002/pola.20529 Search in Google Scholar

[10] Temel G, Enginol B, Aydin M, Balta DK, Arsu N. Photopolymerization and photophysical properties of amine linked benzophenone photoinitiator for free radical polymerization. J Photochem Photobiol A. 2011;219(1):26–31. https://doi.org/10.1016/j.jphotochem.2011.01.012. TemelG EnginolB AydinM BaltaDK ArsuN Photopolymerization and photophysical properties of amine linked benzophenone photoinitiator for free radical polymerization J Photochem Photobiol A 2011 219 1 26 31 https://doi.org/10.1016/j.jphotochem.2011.01.012. 10.1016/j.jphotochem.2011.01.012 Search in Google Scholar

[11] Sipani V, Kirsch A, Scranton AB. Dark cure studies of cationic photopolymerizations of epoxides: Characterization of kinetic rate constants at high conversions. J Polym Sci Part A. 2004;42(17):4409–16. https://doi.org/10.1002/pola.20209. SipaniV KirschA ScrantonAB Dark cure studies of cationic photopolymerizations of epoxides: Characterization of kinetic rate constants at high conversions J Polym Sci Part A 2004 42 17 4409 16 https://doi.org/10.1002/pola.20209. 10.1002/pola.20209 Search in Google Scholar

[12] Noè C, Hakkarainen M, Sangermano M. Cationic UV-curing of epoxidized biobased resins. Polymers. 2020;13(1):89. https://doi.org/10.3390/polym13010089. NoèC HakkarainenM SangermanoM Cationic UV-curing of epoxidized biobased resins Polymers 2020 13 1 89 https://doi.org/10.3390/polym13010089. 10.3390/polym13010089 Search in Google Scholar

[13] Noè C, Malburet S, Milani E, Bouvet-Marchand A, Graillot A, Sangermano M. Cationic UV-curing of epoxidized cardanol derivatives. Polym Int. 2020;69(8):668–74. https://doi.org/10.1002/pi.6031. NoèC MalburetS MilaniE Bouvet-MarchandA GraillotA SangermanoM Cationic UV-curing of epoxidized cardanol derivatives Polym Int 2020 69 8 668 74 https://doi.org/10.1002/pi.6031. 10.1002/pi.6031 Search in Google Scholar

[14] Cho JD, Hong JW. Curing kinetics of UV-initiated cationic photopolymerization of divinyl ether photosensitized by thioxanthone. J Appl Polym Sci. 2010;97(3):1345–51. https://doi.org/10.1002/app.21838. ChoJD HongJW Curing kinetics of UV-initiated cationic photopolymerization of divinyl ether photosensitized by thioxanthone J Appl Polym Sci 2010 97 3 1345 51 https://doi.org/10.1002/app.21838. 10.1002/app.21838 Search in Google Scholar

[15] Heilen W, Herrwerth S. Silicone resins and their combinations. Hannover, Germany: Vincentz Network, 2015. HeilenW HerrwerthS Silicone resins and their combinations Hannover, Germany Vincentz Network 2015 Search in Google Scholar

[16] Bajaj P, Gupta DC. Copolymerization of styrene and acrylonitrile with functional silanes. Eur Polym J. 1979;15(3):271–5. https://doi.org/10.1016/0014-3057(79)90175-7. BajajP GuptaDC Copolymerization of styrene and acrylonitrile with functional silanes Eur Polym J 1979 15 3 271 5 https://doi.org/10.1016/0014-3057(79)90175-7. 10.1016/0014-3057(79)90175-7 Search in Google Scholar

[17] Murias P, Maciejewski H, Galina H. Epoxy resins modified with reactive low molecular weight siloxanes. Eur Polym J. 2012;48(4):769–73. https://doi.org/10.1016/j.eurpolymj.2012.01.009. MuriasP MaciejewskiH GalinaH Epoxy resins modified with reactive low molecular weight siloxanes Eur Polym J 2012 48 4 769 73 https://doi.org/10.1016/j.eurpolymj.2012.01.009. 10.1016/j.eurpolymj.2012.01.009 Search in Google Scholar

[18] Yu Z, Cui A, Zhao P, Wei H, Hu F. Preparation and properties studies of UV-curable silicone modified epoxy resin composite system. J Appl Biomater Fundam Mater. 2018;16(1):170–6. https://doi.org/10.1177/2280800017753053. YuZ CuiA ZhaoP WeiH HuF Preparation and properties studies of UV-curable silicone modified epoxy resin composite system J Appl Biomater Fundam Mater 2018 16 1 170 6 https://doi.org/10.1177/2280800017753053. 10.1177/228080001775305329618261 Search in Google Scholar

[19] Huang B, Han L, Wu B, Chen H, Zhou W, Lu Z. Application of Bis [2-(3,4-epoxycyclohexyl) ethyl]octamethyltetrasiloxane in the preparation of a photosensitive resin for stereolithography 3D printing. J Wuhan Univ Technol. 2019;34(6):236–44. https://doi.org/10.1007/s11595-019-2215-7. HuangB HanL WuB ChenH ZhouW LuZ Application of Bis [2-(3,4-epoxycyclohexyl) ethyl]octamethyltetrasiloxane in the preparation of a photosensitive resin for stereolithography 3D printing J Wuhan Univ Technol 2019 34 6 236 44 https://doi.org/10.1007/s11595-019-2215-7. 10.1007/s11595-019-2215-7 Search in Google Scholar

[20] Khalaf HI, Wady AN, Daham HK. Synthesis and characterization of new optically active poly(amideimide) s derived from n,n′-(pyromellitoyl) bis-l-tyrosine and various diamines. Mater Sci. 2013;31(1):43–51. https://doi.org/10.2478/s13536-012-0077-1. KhalafHI WadyAN DahamHK Synthesis and characterization of new optically active poly(amideimide) s derived from n,n′-(pyromellitoyl) bis-l-tyrosine and various diamines Mater Sci 2013 31 1 43 51 https://doi.org/10.2478/s13536-012-0077-1. 10.2478/s13536-012-0077-1 Search in Google Scholar

[21] Altowyan AS, Ahmed HA, Gomha SM, Mostafa AM. Optical and thermal investigations of new schiff base/ester systems in pure and mixed states. Polymers. 2021;13(11):1687. https://doi.org/10.3390/polym13111687. AltowyanAS AhmedHA GomhaSM MostafaAM Optical and thermal investigations of new schiff base/ester systems in pure and mixed states Polymers 2021 13 11 1687. https://doi.org/10.3390/polym13111687. 10.3390/polym13111687819680934067245 Search in Google Scholar

[22] Suresh J, Karthik S, Arun A. Photocrosslinkable polymer based on 4-(3-(2,4-dichlorophenyl)-3-oxoprop-1-enyl) phenylacrylate: Synthesis, reactivity ratio, and crosslinking studies. Mater Sci. 2016;34(4):834–44. https://doi.org/10.1515/msp-2016-0117. SureshJ KarthikS ArunA Photocrosslinkable polymer based on 4-(3-(2,4-dichlorophenyl)-3-oxoprop-1-enyl) phenylacrylate: Synthesis, reactivity ratio, and crosslinking studies Mater Sci 2016 34 4 834 44 https://doi.org/10.1515/msp-2016-0117. 10.1515/msp-2016-0117 Search in Google Scholar

[23] Shi Y, Ma W, Wang J, Mo J. 2-ethy-4-methylimidazole terminated polyurethane prepolymer as functional latent curing agents for epoxy resin crosslinking. J Macromol Sci Part A. 2019;56(8):750–8. https://doi.org/10.1080/10601325.2019.1586438. ShiY MaW WangJ MoJ 2-ethy-4-methylimidazole terminated polyurethane prepolymer as functional latent curing agents for epoxy resin crosslinking J Macromol Sci Part A 2019 56 8 750 8 https://doi.org/10.1080/10601325.2019.1586438. 10.1080/10601325.2019.1586438 Search in Google Scholar

[24] Rusu MC, Block C, Van Assche G, Van Mele B. Influence of temperature and UV intensity on photo-polymerization reaction studied by photo-DSC. J Thermal Anal Calorimetry. 2012;110(1):287–94. https://doi.org/10.1007/s10973-012-2465-5. RusuMC BlockC Van AsscheG Van MeleB Influence of temperature and UV intensity on photo-polymerization reaction studied by photo-DSC J Thermal Anal Calorimetry 2012 110 1 287 94 https://doi.org/10.1007/s10973-012-2465-5. 10.1007/s10973-012-2465-5 Search in Google Scholar