Analyte | Matrix | Repeatability (RSDr, %) | Within-lab reproducibility (RSDwR, %) | Apparent recovery (%) | Expanded uncertainty (μg kg−1) | CCα (μg kg−1) |
---|---|---|---|---|---|---|
Acepromazine | Kidney | 9.3 | 7.1 | 97.1 | 0.82 | 2.5 |
Urine | 9.8 | 8.3 | 101.6 | 1.04 | 2.5 | |
Azaperol | Kidney | 9.5 | 6.7 | 100.6 | 0.85 | 2.5 |
Urine | 7.7 | 8.1 | 101.0 | 1.10 | 2.5 | |
Azaperone | Kidney | 7.0 | 5.5 | 100.5 | 0.80 | 2.5 |
Urine | 6.0 | 5.2 | 101.2 | 0.67 | 2.5 | |
Carazolol | Kidney | 6.4 | 5.0 | 99.9 | 0.70 | 2.5 |
Urine | 7.4 | 9.8 | 101.6 | 1.43 | 2.5 | |
Chlorpromazine | Kidney | 7.4 | 9.2 | 100.5 | 1.43 | 2.5 |
Urine | 6.6 | 7.3 | 101.3 | 0.96 | 2.5 | |
Haloperidol | Kidney | 8.0 | 10.4 | 97.2 | 1.49 | 2.5 |
Urine | 12.0 | 18.0 | 100.6 | 2.03 | 2.5 | |
Propionylpromazine | Kidney | 8.5 | 8.3 | 97.3 | 1.08 | 2.5 |
Urine | 9.5 | 8.2 | 102.1 | 1.28 | 2.5 | |
Xylazine | Kidney | 9.2 | 10.5 | 99.3 | 1.45 | 2.5 |
Urine | 9.4 | 8.7 | 100.0 | 1.13 | 2.5 |
Analyte | Retention time (min) | Precursor ion (m/z) | Ion transition (m/z) | Declustering potential (eV) | Collision energy (eV) |
---|---|---|---|---|---|
Acepromazine | 2.76 | 326.9 | 86.1 | 100 | 24 |
58.2 | 72 | ||||
Azaperol | 2.61 | 330.1 | 121.0 | 96 | 29 |
312.0 | 21 | ||||
Azaperone | 2.65 | 328.1 | 165.0 | 91 | 27 |
122.9 | 43 | ||||
Carazolol | 2.60 | 299.1 | 116.0 | 96 | 27 |
222.0 | 27 | ||||
Chlorpromazine | 2.85 | 319.0 | 86.0 | 96 | 25 |
245.9 | 31 | ||||
Haloperidol | 2.74 | 376.0 | 165.1 | 110 | 30 |
123.0 | 43 | ||||
Propionylpromazine | 2.82 | 341.0 | 58.0 | 95 | 70 |
86.0 | 25 | ||||
Xylazine | 2.52 | 221.0 | 90.0 | 100 | 27 |
164.1 | 33 | ||||
Acepromazine - D6 | 2.76 | 333.0 | 92.0 | 110 | 25 |
64.0 | 69 | ||||
Azaperol - D4 | 2.61 | 334.1 | 121.0 | 96 | 31 |
153.0 | 39 | ||||
Azaperone - D4 | 2.65 | 332.1 | 169.0 | 101 | 29 |
121.0 | 29 | ||||
Carazolol - D7 | 2.60 | 306.1 | 123.1 | 101 | 27 |
222.0 | 27 | ||||
Chlorpromazine - D6 | 2.85 | 325.0 | 92.1 | 81 | 25 |
245.9 | 33 | ||||
Propionylpromazine - D6 | 2.82 | 347.0 | 92.1 | 100 | 24 |
64.1 | 70 | ||||
Xylazine - D6 | 2.52 | 226.9 | 90.0 | 120 | 29 |
170.0 | 34 |