How different microfilters affect the recovery of eleven EU-regulated mycotoxins

1. Kovač M, Nevistić A, Kovač T, Babić J, Šarić A, Miličević B, Panjičko M, Šarkanj B. Development and validation of an UHPLC-MS/MS method for the simultaneous determination of 11 EU-regulated mycotoxins in selected cereals. J Fungi 2022;8(7):665. doi: 10.3390/jof8070665 Kovač M Nevistić A Kovač T Babić J Šarić A Miličević B Panjičko M Šarkanj B . Development and validation of an UHPLC-MS/MS method for the simultaneous determination of 11 EU-regulated mycotoxins in selected cereals . J Fungi 2022 ; 8 ( 7 ): 665 . doi: 10.3390/jof8070665 Open DOISearch in Google Scholar

2. Turner NW, Subrahmanyam S, Piletsky SA. Analytical methods for determination of mycotoxins: a review. Anal Chim Acta 2009;632:168–80. doi: 10.1016/j.aca.2008.11.010 Turner NW Subrahmanyam S Piletsky SA . Analytical methods for determination of mycotoxins: a review . Anal Chim Acta 2009 ; 632 : 168 – 80 . doi: 10.1016/j.aca.2008.11.010 Open DOISearch in Google Scholar

3. Malachová A, Stránská M, Václavíková M, Elliott CT, Black C, Meneely J, Hajšlová J, Ezekiel CN, Schuhmacher R, Krska R. Advanced LC-MS-based methods to study the co-occurrence and metabolization of multiple mycotoxins in cereals and cereal-based food. Anal Bioanal Chem 2018;410:801–25. doi: 10.1007/s00216-017-0750-7 Malachová A Stránská M Václavíková M Elliott CT Black C Meneely J Hajšlová J Ezekiel CN Schuhmacher R Krska R . Advanced LC-MS-based methods to study the co-occurrence and metabolization of multiple mycotoxins in cereals and cereal-based food . Anal Bioanal Chem 2018 ; 410 : 801 – 25 . doi: 10.1007/s00216-017-0750-7 Open DOISearch in Google Scholar

4. Sulyok M, Berthiller F, Krska R, Schuhmacher R. Development and validation of a liquid chromatography/tandem mass spectrometric method for the determination of 39 mycotoxins in wheat and maize. Rapid Commun Mass Spectrom 2006;20:2649–59. doi: 10.1002/rcm.2640 Sulyok M Berthiller F Krska R Schuhmacher R . Development and validation of a liquid chromatography/tandem mass spectrometric method for the determination of 39 mycotoxins in wheat and maize . Rapid Commun Mass Spectrom 2006 ; 20 : 2649 – 59 . doi: 10.1002/rcm.2640 Open DOISearch in Google Scholar

5. Sulyok M, Krska R, Schuhmacher R. A liquid chromatography/tandem mass spectrometric multi-mycotoxin method for the quantification of 87 analytes and its application to semi-quantitative screening of moldy food samples. Anal Bioanal Chem 2007;389:1505–23. doi: 10.1007/s00216-007-1542-2 Sulyok M Krska R Schuhmacher R . A liquid chromatography/tandem mass spectrometric multi-mycotoxin method for the quantification of 87 analytes and its application to semi-quantitative screening of moldy food samples . Anal Bioanal Chem 2007 ; 389 : 1505 – 23 . doi: 10.1007/s00216-007-1542-2 Open DOISearch in Google Scholar

6. Varga E, Glauner T, Berthiller F, Krska R, Schuhmacher R, Sulyok M. Development and validation of a (semi-)quantitative UHPLC-MS/MS method for the determination of 191 mycotoxins and other fungal metabolites in almonds, hazelnuts, peanuts and pistachios. Anal Bioanal Chem 2013;405:5087–104. doi: 10.1007/s00216-013-6831-3 Varga E Glauner T Berthiller F Krska R Schuhmacher R Sulyok M . Development and validation of a (semi-)quantitative UHPLC-MS/MS method for the determination of 191 mycotoxins and other fungal metabolites in almonds, hazelnuts, peanuts and pistachios . Anal Bioanal Chem 2013 ; 405 : 5087 – 104 . doi: 10.1007/s00216-013-6831-3 Open DOISearch in Google Scholar

7. Malachová A, Sulyok M, Beltrán E, Berthiller F, Krska R. Optimization and validation of a quantitative liquid chromatography-tandem mass spectrometric method covering 295 bacterial and fungal metabolites including all regulated mycotoxins in four model food matrices. J Chromatogr A 2014;1362:145–56. doi: 10.1016/j.chroma.2014.08.037 Malachová A Sulyok M Beltrán E Berthiller F Krska R . Optimization and validation of a quantitative liquid chromatography-tandem mass spectrometric method covering 295 bacterial and fungal metabolites including all regulated mycotoxins in four model food matrices . J Chromatogr A 2014 ; 1362 : 145 – 56 . doi: 10.1016/j.chroma.2014.08.037 Open DOISearch in Google Scholar

8. Kafouris D, Christofidou M, Christodoulou M, Christou E, Ioannou-Kakouri E. A validated UPLC-MS/MS multi-mycotoxin method for nuts and cereals: results of the official control in Cyprus within the EU requirements. Food Agric Immunol 2017;28:90–108. doi: 10.1080/09540105.2016.1228834 Kafouris D Christofidou M Christodoulou M Christou E Ioannou-Kakouri E . A validated UPLC-MS/MS multi-mycotoxin method for nuts and cereals: results of the official control in Cyprus within the EU requirements . Food Agric Immunol 2017 ; 28 : 90 – 108 . doi: 10.1080/09540105.2016.1228834 Open DOISearch in Google Scholar

9. Sulyok M, Stadler D, Steiner D, Krska R. Validation of an LC-MS/MS-based dilute-and-shoot approach for the quantification of > 500 mycotoxins and other secondary metabolites in food crops: challenges and solutions. Anal Bioanal Chem 2020;412:2607–20. doi: 10.1007/s00216-020-02489-9 Sulyok M Stadler D Steiner D Krska R . Validation of an LC-MS/MS-based dilute-and-shoot approach for the quantification of > 500 mycotoxins and other secondary metabolites in food crops: challenges and solutions . Anal Bioanal Chem 2020 ; 412 : 2607 – 20 . doi: 10.1007/s00216-020-02489-9 Open DOISearch in Google Scholar

10. Aichinger G, Živná N, Varga E, Crudo F, Warth B, Marko D. Microfiltration results in the loss of analytes and affects the in vitro genotoxicity of a complex mixture of Alternaria toxins. Mycotoxin Res 2020;36:399–408. doi: 10.1007/s12550-020-00405-9 Aichinger G Živná N Varga E Crudo F Warth B Marko D . Microfiltration results in the loss of analytes and affects the in vitro genotoxicity of a complex mixture of Alternaria toxins . Mycotoxin Res 2020 ; 36 : 399 – 408 . doi: 10.1007/s12550-020-00405-9 Open DOISearch in Google Scholar

11. Carlson M, Thompson RD. Analyte loss due to membrane filter adsorption as determined by high-performance liquid chromatography. J Chromatogr Sci 2000;38:77–83. doi: 10.1093/chromsci/38.2.77 Carlson M Thompson RD . Analyte loss due to membrane filter adsorption as determined by high-performance liquid chromatography . J Chromatogr Sci 2000 ; 38 : 77 – 83 . doi: 10.1093/chromsci/38.2.77 Open DOISearch in Google Scholar

12. Zhao L, Long W. Syringe Filter Suitability for Sample Preparation in Drug Assays. Agilent Technologies 2013 [displayed 15 march 2023]. Available at https://www.agilent.com/cs/library/applications/5991-2409EN.pdf Zhao L Long W . Syringe Filter Suitability for Sample Preparation in Drug Assays . Agilent Technologies 2013 [displayed 15 march 2023]. Available at https://www.agilent.com/cs/library/applications/5991-2409EN.pdf Search in Google Scholar

13. European Commission. Commission Regulation (EC) No 1881/2006 of 19 December 2006 setting maximum levels for certain contaminants in foodstuffs [displayed 15 March 2023]. Available at https://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2006:364:0005:0024:EN:PDF European Commission . Commission Regulation (EC) No 1881/2006 of 19 December 2006 setting maximum levels for certain contaminants in foodstuffs [displayed 15 March 2023] . Available at https://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2006:364:0005:0024:EN:PDF Search in Google Scholar

14. European Commission. Directive 2002/32/EC of the European Parliament and of the Council of 7 May 2002 on undesirable substances in animal feed [displayed 15 March 2023]. Available at https://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=CONSLEG:2002L0032:20061020:EN:PDF European Commission . Directive 2002/32/EC of the European Parliament and of the Council of 7 May 2002 on undesirable substances in animal feed [displayed 15 March 2023] . Available at https://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=CONSLEG:2002L0032:20061020:EN:PDF Search in Google Scholar

15. Frenich AG, Vidal JLM, Romero-González R, Aguilera-Luiz M del M. Simple and high-throughput method for the multimycotoxin analysis in cereals and related foods by ultra-high performance liquid chromatography/tandem mass spectrometry. Food Chem 2009;117:705–12. doi: 10.1016/j.foodchem.2009.04.045 Frenich AG Vidal JLM Romero-González R Aguilera-Luiz M del M . Simple and high-throughput method for the multimycotoxin analysis in cereals and related foods by ultra-high performance liquid chromatography/tandem mass spectrometry . Food Chem 2009 ; 117 : 705 – 12 . doi: 10.1016/j.foodchem.2009.04.045 Open DOISearch in Google Scholar

16. De Santis B, Debegnach F, Gregori E, Russo S, Marchegiani F, Moracci G, Brera C. Development of a LC-MS/MS method for the multi-mycotoxin determination in composite cereal-based samples. Toxins (Basel) 2017;9(5):169. doi: 10.3390/toxins9050169 De Santis B Debegnach F Gregori E Russo S Marchegiani F Moracci G Brera C . Development of a LC-MS/MS method for the multi-mycotoxin determination in composite cereal-based samples . Toxins (Basel) 2017 ; 9 ( 5 ): 169 . doi: 10.3390/toxins9050169 Open DOISearch in Google Scholar

17. Carballo D, Font G, Ferrer E, Berrada H. Evaluation of mycotoxin residues on ready-to-eat food by chromatographic methods coupled to mass spectrometry in tandem. Toxins (Basel) 2018;10(6):243. doi: 10.3390/toxins10060243 Carballo D Font G Ferrer E Berrada H . Evaluation of mycotoxin residues on ready-to-eat food by chromatographic methods coupled to mass spectrometry in tandem . Toxins (Basel) 2018 ; 10 ( 6 ): 243 . doi: 10.3390/toxins10060243 Open DOISearch in Google Scholar