<abstract xmlns="http://www.w3.org/1999/xhtml"> Shuttle-like BaMoO4 microstructure has been successfully synthesized from Ba(N03)2·4H20 and Na2MoO4·2H2O as starting materials in ethylene glycol solvent containing 20 mL 5 M NaOH by microwave radiation at 180 W for 30 min. The as- synthesized BaMoO4 product was characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, Raman spectrophotometry, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and photolumines­cence (PL) spectroscopy. XRD patterns revealed that the products was tetragonal BaMoO4 phase. SEM and TEM characteriza­tion showed that the product had a shuttle-like BaMoO4 microstructure. PL of the shuttle-like BaMoO4 microstructure showed a maximum emission at 466 nm excited by 280 nm wavelength. </abstract>

Shuttle-like BaMoO4 microstructure has been successfully synthesized from Ba(N03)2·4H20 and Na2MoO4·2H2O as starting materials in ethylene glycol solvent containing 20 mL 5 M NaOH by microwave radiation at 180 W for 30 min. The as- synthesized BaMoO4 product was characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, Raman spectrophotometry, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and photolumines­cence (PL) spectroscopy. XRD patterns revealed that the products was tetragonal BaMoO4 phase. SEM and TEM characteriza­tion showed that the product had a shuttle-like BaMoO4 microstructure. PL of the shuttle-like BaMoO4 microstructure showed a maximum emission at 466 nm excited by 280 nm wavelength.

Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO4 microstructure

Department of Materials Science and Technology, Faculty of Science, Prince of Songkla University, Hat Yai, Songkhla 90112, Thailand

Electron Microscopy Research and Service Center, Faculty of Science, Chiang Mai University, Chiang Mai 50200, Thailand

Department of Chemistry, Faculty of Science, Chiang Mai University, Chiang Mai 50200, Thailand

Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200, Thailand

Materials Science Research Center, Faculty of Science, Chiang Mai University, Chiang Mai 50200, Thailand

Materials Science-Poland

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO microstructure

Shuttle-like BaMoO4 microstructure has been successfully synthesized from Ba(N03)2·4H20 and Na2MoO4·2H2O as starting materials in ethylene glycol solvent...

Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO₄ microstructure

Publié en ligne: 30 août 2016

Pages: 537 - 540

Reçu: 28 oct. 2014

Accepté: 08 juin 2015

DOI: https://doi.org/10.1515/msp-2015-0093

Mots clés
BaMoO4, shuttle-like particles, luminescence

© 2016

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO4 microstructure

Publié en ligne: 30 août 2016

Pages: 537 - 540

Reçu: 28 oct. 2014

Accepté: 08 juin 2015

DOI: https://doi.org/10.1515/msp-2015-0093

Mots clésBaMoO4, shuttle-like particles, luminescence

© 2016

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO₄ microstructure

Mots clés
BaMoO4, shuttle-like particles, luminescence