Factors influencing preparation of polyaniline doped with hydrochloric acid
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19 dic 2014
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Publicado en línea: 19 dic 2014
Páginas: 521 - 525
DOI: https://doi.org/10.2478/s13536-014-0251-8
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© 2014 Wroclaw University of Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.
Factors influencing the reaction of chemical polymerization during aniline doping with hydrochloric acid (HCl) have been studied in this work. The optimal parameters for the preparation of polyaniline were determined as follows: aniline concentration - 4 mass %, molar ratios of oxidant (NH4)2S2O8:aniline - 1.2:1 and 1.3:1, the concentration of dopant - 1 mol/L. Fourier transform infrared spectroscopy (FT-IR) was applied to characterize the structure of polyaniline.