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Non-isothermal melt- and cold-crystallization, melting process, and optical and mechanical properties of PLLA: the effect of TAPH


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Fig. 1.

Synthetic route of TAPH
Synthetic route of TAPH

Fig. 2.

DSC cooling curves of pure PLLA and PLLA/TAPH from 190°C at a rate of 1°C/min
DSC cooling curves of pure PLLA and PLLA/TAPH from 190°C at a rate of 1°C/min

Fig. 3.

DSC cooling curves of PLLA/TAPH at different rates (2.5°C/min, 5°C/min, 10°C/min, and 20°C/min)
DSC cooling curves of PLLA/TAPH at different rates (2.5°C/min, 5°C/min, 10°C/min, and 20°C/min)

Fig. 4.

DSC heating curves of PLLA/TAPH at different rates (1°C/min, 2.5°C/min, and 5°C/min)
DSC heating curves of PLLA/TAPH at different rates (1°C/min, 2.5°C/min, and 5°C/min)

Fig. 5.

Melting processes of PLLA/TAPH at different heating rates (1°C/min, 2°C/min, 4°C/min, 8°C/min, and 16° C/min) after melt crystallization
Melting processes of PLLA/TAPH at different heating rates (1°C/min, 2°C/min, 4°C/min, 8°C/min, and 16° C/min) after melt crystallization

Fig. 6.

DSC melting curves of PLLA/TAPH after isothermal crystallization at different temperatures for 180 min
DSC melting curves of PLLA/TAPH after isothermal crystallization at different temperatures for 180 min

Fig. 7.

Transparency of pure PLLA and PLLA/TAPH
Transparency of pure PLLA and PLLA/TAPH

Fig. 8.

Effect of TAPH loading on the mechanical properties of PLLA
Effect of TAPH loading on the mechanical properties of PLLA
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Temas de la revista:
Materials Sciences, other, Nanomaterials, Functional and Smart Materials, Materials Characterization and Properties