Simultaneous determination of sulfonamides, trimethoprim, amoxicillin and tylosin in medicated feed by high performance liquid chromatography with mass spectrometry
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Benito-Pena E., Urrac J.L., Moreno-Bondi M.C.: Quantitative determination of penicillin V and amoxicillin in feed samples by pressurised liquid extraction and liquid chromatography with ultraviolet detection. J Pharm Biomed Anal 2009, 49, 289–294, doi: 10.1016/j.jpba.2008.11.016.Benito-PenaE.UrracJ.L.Moreno-BondiM.C.:Quantitative determination of penicillin V and amoxicillin in feed samples by pressurised liquid extraction and liquid chromatography with ultraviolet detection.2009,49,289–294, doi:10.1016/j.jpba.2008.11.016.Open DOISearch in Google Scholar
Borràs S., Companyó R., Guiteras J.: Analysis of Sulfonamides in Animal Feeds by Liquid Chromatography with Fluorescence Detection. J Agric Food Chem 2011, 59, 5240–5247, doi: 10.1021/jf2005595.BorràsS.CompanyóR.GuiterasJ.:Analysis of Sulfonamides in Animal Feeds by Liquid Chromatography with Fluorescence Detection.2011,59,5240–5247, doi:10.1021/jf2005595.Open DOISearch in Google Scholar
Commission Implementing Regulation (EU) 2021/808 of 22 March 2021 on the performance of analytical methods for residues of pharmacologically active substances used in food-producing animals and on the interpretation of results as well as on the methods to be used for sampling and repealing Decisions 2002/657/EC and 98/179/EC..Search in Google Scholar
Croubels S., Wassink P., De Backer P.: Simultaneous determination of sulfadiazine and trimethoprim in animal feed by liquid chromatography with UV and tandem mass spectrometric detection. Anal Chim Acta 2002, 473, 183–194, doi: 10.1016/S0003-2670(02)00976-5.CroubelsS.WassinkP.De BackerP.:Simultaneous determination of sulfadiazine and trimethoprim in animal feed by liquid chromatography with UV and tandem mass spectrometric detection.2002,473,183–194, doi:10.1016/S0003-2670(02)00976-5.Open DOISearch in Google Scholar
De Baere S., De Backer P.: Quantitative determination of amoxicillin in animal feed using liquid chromatography with tandem mass spectrometric detection. Anal Chim Acta 2007, 586, 319–325, doi: 10.1016/j.aca.2006.10.036.De BaereS.De BackerP.:Quantitative determination of amoxicillin in animal feed using liquid chromatography with tandem mass spectrometric detection.2007,586,319–325, doi:10.1016/j.aca.2006.10.036.Open DOISearch in Google Scholar
European Medicines Agency, European Surveillance of Veterinary Antimicrobial Consumption (ESVAC) project: Sales of veterinary antimicrobial agents in 31 European countries in 2021. Trends from 2010 to 2021. Twelfth ESVAC report. EMA, Amsterdam, 2022, https://www.ema.europa.eu/en/documents/report/sales-veterinary-antimicrobial-agents-31-european-countries-2021-trends-2010-2021-twelfh-esvac-report_en.pdf.European Medicines Agency,European Surveillance of Veterinary Antimicrobial Consumption (ESVAC) project: Sales of veterinary antimicrobial agents in 31 European countries in 2021..EMA,Amsterdam,2022, https://www.ema.europa.eu/en/documents/report/sales-veterinary-antimicrobial-agents-31-european-countries-2021-trends-2010-2021-twelfh-esvac-report_en.pdf.Search in Google Scholar
Gamba V., Dusi G.: Liquid chromatography with fluorescence detection of amoxicillin and ampicillin in feeds using pre-column derivatization. Anal Chim Acta 2003, 483, 69–72, doi: 10.1016/S0003-2670(02)01475-7.GambaV.DusiG.:Liquid chromatography with fluorescence detection of amoxicillin and ampicillin in feeds using pre-column derivatization.2003,483,69–72, doi:10.1016/S0003-2670(02)01475-7.Open DOISearch in Google Scholar
Gavilán R.E., Nebot C., Miranda J.M., Martín-Gómez Y., Vázquez-Belda B., Franco C.M., Cepeda A.: Analysis of Tetracyclines in Medicated Feed for Food Animal Production by HPLC-MS/MS. Antibiotics 2016, 5, 1, doi: 10.3390/antibiotics5010001.GavilánR.E.NebotC.MirandaJ.M.Martín-GómezY.Vázquez-BeldaB.FrancoC.M.CepedaA.:Analysis of Tetracyclines in Medicated Feed for Food Animal Production by HPLC-MS/MS.2016,5,1, doi:10.3390/antibiotics5010001.Open DOISearch in Google Scholar
International Council for Harmonisation of Technical Requirements for Pharmaceuticals for Human Use (ICH): Q2B. Validation of Analytical Procedures: Methodology. ICH Secretariat, Geneva, 1997.International Council for Harmonisation of Technical Requirements for Pharmaceuticals for Human Use (ICH): Q2B..ICH Secretariat,Geneva,1997.Search in Google Scholar
Kochansky J.: Evaluation of purification schemes in the determination of tylosin in honey using high performance liquid chromatography. J Apicultural Res 2004, 43, 60–64, doi: 10.1080/00218839.2004.11101112.KochanskyJ.:Evaluation of purification schemes in the determination of tylosin in honey using high performance liquid chromatography.2004,43,60–64, doi:10.1080/00218839.2004.11101112.Open DOISearch in Google Scholar
Krasucka D., Mitura A., Cybulski W., Kos K., Pietroń W.: Tiamulin hydrogen fumarate--veterinary uses and HPLC method of determination in premixes and medicated feedingstuffs. Acta Pol Pharm 2010, 67, 682–685.KrasuckaD.MituraA.CybulskiW.KosK.PietrońW.:Tiamulin hydrogen fumarate--veterinary uses and HPLC method of determination in premixes and medicated feedingstuffs.2010,67,682–685.Search in Google Scholar
Luo W., Hansen E.B. Jr., Ang C.Y.W., Deck J., Freeman J.P., Thompson H.C. Jr.: Simultaneous determination of amoxicillin and ampicillin in bovine milk by HPLC with fluorescence detection. J Agri Food Chem 1997, 45, 1264–1268, doi: 10.1021/jf960739l.LuoW.HansenE.B.JrAngC.Y.W.DeckJ.FreemanJ.P.ThompsonH.C.Jr.:Simultaneous determination of amoxicillin and ampicillin in bovine milk by HPLC with fluorescence detection.1997,45,1264–1268, doi:10.1021/jf960739l.Open DOISearch in Google Scholar
Patyra E., Kowalczyk E., Kwiatek K.: Determination of chlorotetracycline and doxycycline in medicated feedingstuffs by liquid chromatography. Bull Vet Inst Pulawy 2012, 56, 329–333, doi: 10.2478/v10213-012-0058-5.PatyraE.KowalczykE.KwiatekK.:Determination of chlorotetracycline and doxycycline in medicated feedingstuffs by liquid chromatography.2012,56,329–333, doi:10.2478/v10213-012-0058-5.Open DOISearch in Google Scholar
Patyra E., Kowalczyk E., Kwiatek K.: Development and validation method for the determination of selected tetracyclines in animal medicated feedingstuffs with the use of micellar liquid chromatography. Anal Bioanal Chem 2013, 405, 6799–6806, doi: 10.1007/s00216-013-7117-5.PatyraE.KowalczykE.KwiatekK.:Development and validation method for the determination of selected tetracyclines in animal medicated feedingstuffs with the use of micellar liquid chromatography.2013,405,6799–6806, doi:10.1007/s00216-013-7117-5.Open DOISearch in Google Scholar
Patyra E., Kwiatek K.: Analytical procedure for the determination of tetracyclines in medicated feedingstuffs by liquid chromatography-mass spectrometry. J Vet Res 2016, 60, 35–41, doi: 10.1515/jvetres-2016-0006.PatyraE.KwiatekK.:Analytical procedure for the determination of tetracyclines in medicated feedingstuffs by liquid chromatography-mass spectrometry.2016,60,35–41, doi:10.1515/jvetres-2016-0006.Open DOISearch in Google Scholar
Patyra E., Kwiatek K.: HPLC-DAD analysis of florfenicol and thiamphenicol in medicated feedingstuffs. Food Addit Contam Part A. 2019, 36, 1184–1190, doi: 10.1080/19440049.2019.1619943.PatyraE.KwiatekK.:HPLC-DAD analysis of florfenicol and thiamphenicol in medicated feedingstuffs..2019,36,1184–1190, doi:10.1080/19440049.2019.1619943.Open DOISearch in Google Scholar
Patyra E., Kwiatek K.: Application of Micellar Mobile Phase for Quantification of Sulfonamides in Medicated Feeds by HPLC-DAD. Molecules 2021, 26, 3791, doi: 10.3390/molecules26133791.PatyraE.KwiatekK.:Application of Micellar Mobile Phase for Quantification of Sulfonamides in Medicated Feeds by HPLC-DAD.2021,26,3791, doi:10.3390/molecules26133791.Open DOISearch in Google Scholar
Patyra E., Kwiatek K.: In-house validation method for quantification of amoxicillin in medicated feedingstuffs with the use of HPLC-DAD technique. J Vet Res 2020, 64, 433–438, doi: 10.2478/jvetres-2020-0044.PatyraE.KwiatekK.:In-house validation method for quantification of amoxicillin in medicated feedingstuffs with the use of HPLC-DAD technique.2020,64,433–438, doi:10.2478/jvetres-2020-0044.Open DOISearch in Google Scholar
Patyra E., Nebot C., Gavilán R.E., Cepeda A., Kwiatek K.: Development and validation of an LC-MS/MS method for the quantification of tiamulin, trimethoprim, tylosin, sulfadiazine and sulfamethazine in medicated feed. Food Addit Contam Part A 2018, 35, 882–891, doi: 10.1080/19440049.2018.1426887.PatyraE.NebotC.GavilánR.E.CepedaA.KwiatekK.:Development and validation of an LC-MS/MS method for the quantification of tiamulin, trimethoprim, tylosin, sulfadiazine and sulfamethazine in medicated feed.2018,35,882–891, doi:10.1080/19440049.2018.1426887.Open DOISearch in Google Scholar
Pietroń W., Cybulski W., Kos K., Mitura A.: Analytical procedure for the determination of tylosin A in feedingstuffs by liquid chromatography–ultraviolet detection. Bull Vet Inst Pulawy 2011, 55, 725–729.PietrońW.CybulskiW.KosK.MituraA.:Analytical procedure for the determination of tylosin A in feedingstuffs by liquid chromatography–ultraviolet detection.2011,55,725–729.Search in Google Scholar
Pietroń W., Cybulski W., Krasucka D., Mitura A., Kos K., Antczak M.: Determination of five sulfonamides in medicated feedingstuffs by liquid chromatography with ultraviolet detection. Bull Vet Inst Pulawy 2013, 57, 545–552, doi: 10.2478/bvip-2013-0094.PietrońW.CybulskiW.KrasuckaD.MituraA.KosK.AntczakM.:Determination of five sulfonamides in medicated feedingstuffs by liquid chromatography with ultraviolet detection.2013,57,545–552, doi:10.2478/bvip-2013-0094.Open DOISearch in Google Scholar
Pietroń W., Woźniak A., Pasik K., Cybulski W., Krasucka D.: Amphenicols stability in medicated feed – development and validation of liquid chromatography method. Bull Vet Inst Pulawy 2014, 58, 621–629, doi: 10.2478/bvip-2014-0095.PietrońW.WoźniakA.PasikK.CybulskiW.KrasuckaD.:Amphenicols stability in medicated feed – development and validation of liquid chromatography method.2014,58,621–629, doi:10.2478/bvip-2014-0095.Open DOISearch in Google Scholar
Przeniosło-Siwczyńska M., Kowalczyk E., Kwiatek K.: Determination of sulfaguanidine in medicated feedingstuffs by liquid chromatography-mass spectrometry. Bull Vet Inst Puławy 2011, 55, 717–720.Przeniosło-SiwczyńskaM.KowalczykE.KwiatekK.:Determination of sulfaguanidine in medicated feedingstuffs by liquid chromatography-mass spectrometry.2011,55,717–720.Search in Google Scholar
Regulation (EU) 2019/4 of the European Parliament and of the Council of 11 December 2018 on the manufacture, placing on the market and use of medicated feed, amending Regulation (EC) No. 183/2005 of the European Parliament and of the Council and repealing Council Directive 90/167/EEC..Search in Google Scholar
Smallidge R.L., Kendrick A.: Determination of sulfamethazine in swine and cattle feed by reserved-phase liquid chromatography with post-column derivatization: collaborative study. J AOAC Inter 2000, 83, 260–268, doi: 10.1093/jaoac/83.2.260.SmallidgeR.L.KendrickA.:Determination of sulfamethazine in swine and cattle feed by reserved-phase liquid chromatography with post-column derivatization: collaborative study.2000,83,260–268, doi:10.1093/jaoac/83.2.260.Open DOISearch in Google Scholar
Yang J.J., Sun G.Z., Qian M.R., Huang L.L., Ke X.B., Yang B.: Development of a high-performance liquid chromatography method for the determination of florfenicol in animal feedstuffs. J Chrom B 2017, 1068-1069, 9–14, doi: 10.1016/j.jchromb.2017.09.045.YangJ.J.SunG.Z.QianM.R.HuangL.L.KeX.B.YangB.:Development of a high-performance liquid chromatography method for the determination of florfenicol in animal feedstuffs.2017,1068-1069,9–14, doi:10.1016/j.jchromb.2017.09.045.Open DOISearch in Google Scholar