<abstract xmlns="http://www.w3.org/1999/xhtml"><p>A gas-chromatographic procedure using the electron-capture detector is presented. By fractionation of cigarette smoke on silica gel, followed by gas-chromatographic analysis of the fractions, fifteen polycyclic aromatic hydrocarbons were identified. Application of this procedure to quantitative analysis was demonstrated in the case of benzo[a]pyrene. An analysis for benzo[a]pyrene in cigarette smoke which utilizes paper-chromatographic separation and fluorescence measurements is also presented. This procedure, which gives good precision with a 20-cigarette sample, represents a great simplification of existing methods. </p></abstract>

A gas-chromatographic procedure using the electron-capture detector is presented. By fractionation of cigarette smoke on silica gel, followed by gas-chromatographic analysis of the fractions, fifteen polycyclic aromatic hydrocarbons were identified. Application of this procedure to quantitative analysis was demonstrated in the case of benzo[a]pyrene. An analysis for benzo[a]pyrene in cigarette smoke which utilizes paper-chromatographic separation and fluorescence measurements is also presented. This procedure, which gives good precision with a 20-cigarette sample, represents a great simplification of existing methods.

Analysis of Polycyclic Hydrocarbons

Guvernator III GC, Edmonds MD, Bavley A Affiliation(s):	Philip Morris Inc., Richmond, Va., USA

Contributions to Tobacco & Nicotine Research

This article is distributed under the terms of the Creative Commons Attribution Non-Commercial License, which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.

{"article-title":"Analysis of Polycyclic Hydrocarbons"}

A gas-chromatographic procedure using the electron-capture detector is presented. By fractionation of cigarette smoke on silica gel, followed by...

Analysis of Polycyclic Hydrocarbons

Publicado en línea: 13 jun 2014

Páginas: 278 - 284

DOI: https://doi.org/10.2478/cttr-2013-0119

© Beiträge zur Tabakforschung International

This article is distributed under the terms of the Creative Commons Attribution Non-Commercial License, which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.