<abstract xmlns="http://www.w3.org/1999/xhtml">Two different absorption correction methods were compared in order to find out which method is preferable to improve solving and refining a crystal structure. Experiments were performed on the crystal of a tetrakis(μ2-acetato)-diaqua-di-copper(II) complex. The first correction method used was the numerical absorption correction with the aid of a crystal-shape model, and the other was the semi-empirical one, applying scaling routines to the intensity data.</abstract>

Two different absorption correction methods were compared in order to find out which method is preferable to improve solving and refining a crystal structure. Experiments were performed on the crystal of a tetrakis(μ2-acetato)-diaqua-di-copper(II) complex. The first correction method used was the numerical absorption correction with the aid of a crystal-shape model, and the other was the semi-empirical one, applying scaling routines to the intensity data.

Comparison of different absorption corrections on the model structure of tetrakis(μ2-acetato)-diaqua-di-copper(II)

Faculty of Chemical and Food Technology, Slovak Technical University, Radlinského 9, SK-812 37, Bratislava,

STOE & Cie GmbH, Hilpertstrasse 10, D-64295, Darmstadt,

Acta Chimica Slovaca

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Comparison of different absorption corrections on the model structure of tetrakis(μ-acetato)-diaqua-di-copper(II)

Two different absorption correction methods were compared in order to find out which method is preferable to improve solving and refining a crystal structure....

Comparison of different absorption corrections on the model structure of tetrakis(μ₂-acetato)-diaqua-di-copper(II)

Publicado en línea: 08 dic 2016

Páginas: 136 - 140

DOI: https://doi.org/10.1515/acs-2016-0023

Palabras clave
Absorption correction, crystal structure, accuracy

© 2016 Faculty of Chemical and Food Technology, Slovak University of Technology in Bratislava

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Comparison of different absorption corrections on the model structure of tetrakis(μ2-acetato)-diaqua-di-copper(II)

Publicado en línea: 08 dic 2016

Páginas: 136 - 140

DOI: https://doi.org/10.1515/acs-2016-0023

Palabras claveAbsorption correction, crystal structure, accuracy

© 2016 Faculty of Chemical and Food Technology, Slovak University of Technology in Bratislava

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Comparison of different absorption corrections on the model structure of tetrakis(μ₂-acetato)-diaqua-di-copper(II)

Palabras clave
Absorption correction, crystal structure, accuracy