Dh k l = Calculated crystallize size [nm] | ||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|
h k l | Sample 1 | Sample 2 | Sample 3 | Sample 4 | ||||||||
2θ | FWHM | Dh k l | 2θ | FWHM | Dh k l | 2θ | FWHM | Dh k l | 2θ | FWHM | Dh k l | |
(1 1 1) | 18.34 | 0.18 | 46.72 | 17.52 | 0.30 | 28 | 17.35 | 0.30 | 27.99 | 18.41 | 0.18 | 46.72 |
(2 2 0) | 30.15 | 0.12 | 71.64 | 30.36 | 0.24 | 35.84 | 30.19 | 0.24 | 35.82 | 30.18 | 0.12 | 71.65 |
(3 1 1) | 35.50 | 0.18 | 48.42 | 35.60 | 0.30 | 29.06 | 35.61 | 0.30 | 29.61 | 35.55 | 0.18 | 48.43 |
(4 0 0) | 43.13 | 0.18 | 49.59 | 43.32 | 0.30 | 29.77 | 43.20 | 0.30 | 29.76 | 43.19 | 0.30 | 29.76 |
(4 2 2) | 53.49 | 0.18 | 51.64 | 53.68 | 0.18 | 51.67 | 53.52 | 0.18 | 51.64 | 53.52 | 0.30 | 30.99 |
(5 1 1) | 56.99 | 0.12 | 78.7 | 57.27 | 0.24 | 39.40 | 57.24 | 0.24 | 39.40 | 57.06 | 0.12 | 78.73 |
(4 4 0) | 62.57 | 0.12 | 80.93 | 62.86 | 0.24 | 40.53 | 62.90 | 0.24 | 40.54 | 62.65 | 0.24 | 40.48 |
(6 2 0) | 70.97 | 0.18 | 56.63 | 71.39 | 0.30 | 34.06 | 71.18 | 0.12 | 85.05 | 71.03 | 0.18 | 56.65 |
(6 2 2) | 74.03 | 0.24 | 43.31 | 74.33 | 0.24 | 43.39 | 74.56 | 0.24 | 43.46 | 74.08 | 0.12 | 86.64 |