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(0 0 2)-oriented growth and morphologies of ZnO thin films prepared by sol-gel method

Dongyun Guo
Dongyun Guo
, 
Yang Ju
Yang Ju
, 
Chengju Fu
Chengju Fu
, 
Zhixiong Huang
Zhixiong Huang
 und 
Lianmeng Zhang
Lianmeng Zhang
   | 21. Sept. 2016
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Article Category: Research Article
Online veröffentlicht: 21. Sept. 2016
Seitenbereich: 555 - 563
Eingereicht: 02. Nov. 2015
Akzeptiert: 02. Juni 2016
DOI: https://doi.org/10.1515/msp-2016-0076
Schlüsselwörter
© 2016 Dongyun Guo et al., published by Sciendo
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.

Fig. 1

Process flow chart for preparation of ZnO thin films.
Process flow chart for preparation of ZnO thin films.

Fig. 2

XRD patterns of ZnO thin films obtained using Zn-solutions with 2-(methylamino)ethanol and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.
XRD patterns of ZnO thin films obtained using Zn-solutions with 2-(methylamino)ethanol and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.

Fig. 3

Surface morphology of ZnO thin film using Zn-solution with 2-(methylamino)ethanol and ethanol baked at 160 °C.
Surface morphology of ZnO thin film using Zn-solution with 2-(methylamino)ethanol and ethanol baked at 160 °C.

Fig. 4

Surface morphologies of ZnO thin films using Zn-solutions with 2-(methylamino)ethanol and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.
Surface morphologies of ZnO thin films using Zn-solutions with 2-(methylamino)ethanol and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.

Fig. 5

XRD patterns of ZnO thin films using Zn-solutions with monoethanolamine and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.
XRD patterns of ZnO thin films using Zn-solutions with monoethanolamine and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.

Fig. 6

Surface morphologies of ZnO thin films using Zn-solutions with monoethanolamine and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.
Surface morphologies of ZnO thin films using Zn-solutions with monoethanolamine and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.

Fig. 7

XRD patterns of ZnO thin films using Zn-solutions with diethanolamine and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.
XRD patterns of ZnO thin films using Zn-solutions with diethanolamine and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.

Fig. 8

Surface morphologies of ZnO thin films using Zn-solutions with diethanolamine and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.
Surface morphologies of ZnO thin films using Zn-solutions with diethanolamine and different solvents: (a) methanol, (b) ethanol, (c) n-propanol and (d) 2-methoxyethanol baked at different temperatures.

Atmospheric boiling temperature of the solvents and ligands.

Boiling temperatures [°C]
Solvent
Methanol64.7
Ethanol78
n-propanol97
2-methoxyethanol124
Ligand
2-(methylamino)ethanol159
Monoethanolamine170
Diethanolamine268

The details of solutions.

No. of solutionLigandSolvent
12-(methylamino)ethanolMethanol
2Ethanol
3n-propanol
42-methoxyethanol
5MonoethanolamineMethanol
6Ethanol
7n-propanol
82-methoxyethanol
9DiethanolamineMethanol
10Ethanol
11n-propanol
122-methoxyethanol
eISSN:
2083-134X
Sprache:
Englisch
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Materialwissenschaft, andere, Nanomaterialien, Funktionelle und Intelligente Materialien, Charakterisierung und Eigenschaften von Materialien
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