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Fig. 1

A – tectonic map with major tectonic units of the Alps, Carpathians and Dinarides (Schmid et al., 2016), with the position of the Slavonian Mts. (Croatia) marked by a black rectangle (B). B – The geology of the crystalline basement rocks of the Slavonian Mts. A simplified geological outline of the Slavonian Mts. (Psunj, Papuk and Krnidja) (according to Jamičić, 2001) with sampled locations: PSG-1 Omanovac Quarry (Psunj Mt.), 2PPG-32 Šandrovac Quarry (NW Papuk Mt.) and HEG-31 Kišeljevac Creek (S slope of Papuk Mt.). Legend: 1 – Graniotoids (G), 2 – Migmatites (Mi), 3 – Biotite-muscovite gneiss (Gmb), 4 – garnet-staurolite gneiss, kyanite gneiss, sillimanite gneiss, amphibolite, metagabbro, amphibole-schist, chlorite-sericite schist and flaser granitoids, and other different types of granitoids with marble. C – Schematic drawing of three series of basement rocks: the Psunj-Krndija, Papuk and Radlovac Complexes.
A – tectonic map with major tectonic units of the Alps, Carpathians and Dinarides (Schmid et al., 2016), with the position of the Slavonian Mts. (Croatia) marked by a black rectangle (B). B – The geology of the crystalline basement rocks of the Slavonian Mts. A simplified geological outline of the Slavonian Mts. (Psunj, Papuk and Krnidja) (according to Jamičić, 2001) with sampled locations: PSG-1 Omanovac Quarry (Psunj Mt.), 2PPG-32 Šandrovac Quarry (NW Papuk Mt.) and HEG-31 Kišeljevac Creek (S slope of Papuk Mt.). Legend: 1 – Graniotoids (G), 2 – Migmatites (Mi), 3 – Biotite-muscovite gneiss (Gmb), 4 – garnet-staurolite gneiss, kyanite gneiss, sillimanite gneiss, amphibolite, metagabbro, amphibole-schist, chlorite-sericite schist and flaser granitoids, and other different types of granitoids with marble. C – Schematic drawing of three series of basement rocks: the Psunj-Krndija, Papuk and Radlovac Complexes.

Fig. 2

Representative sample (PSG-1) from Omanovac Quarry (Psunj Mt., Croatia): A – macrophotography (R coin = 16 mm); B–D microphotographs (crossed nicols). Abbreviations: Qtz – quartz, Kfs – K-feldspar, Pl – plagioclase, Amp – amphibole.
Representative sample (PSG-1) from Omanovac Quarry (Psunj Mt., Croatia): A – macrophotography (R coin = 16 mm); B–D microphotographs (crossed nicols). Abbreviations: Qtz – quartz, Kfs – K-feldspar, Pl – plagioclase, Amp – amphibole.

Fig. 3

Representative sample (2PPG-32) from Šandrovac Quarry (Papuk Mt., Croatia): A – macrophotography (scale in cm); B–D micro-photographs (crossed nicols). Abbreviations: Qtz – quartz, Kfs – K-feldspar, Pl – plagioclase, Bi – biotite, Ms - muscovite.
Representative sample (2PPG-32) from Šandrovac Quarry (Papuk Mt., Croatia): A – macrophotography (scale in cm); B–D micro-photographs (crossed nicols). Abbreviations: Qtz – quartz, Kfs – K-feldspar, Pl – plagioclase, Bi – biotite, Ms - muscovite.

Fig. 4

Representative sample (HEG-31) from Kišeljevac Creek (Papuk Mt., Croatia): A–D microphotographs (crossed nicols). Abbreviations: Qtz – quartz, Kfs – K-feldspar, Bt – biotite.
Representative sample (HEG-31) from Kišeljevac Creek (Papuk Mt., Croatia): A–D microphotographs (crossed nicols). Abbreviations: Qtz – quartz, Kfs – K-feldspar, Bt – biotite.

Fig. 5

Cathodoluminescence images of dated zircon crystals separated from the amphibole monzogranite (PSG-1) from Omanovac Quarry, Psunj Mt., Croatia. The white rectangles and circles mark the in-situ laser-ablation track used for U/Pb dating, (ø = 10–15–20 μm), and they are not in scale. Measurement numbers are listed in Table 1.
Cathodoluminescence images of dated zircon crystals separated from the amphibole monzogranite (PSG-1) from Omanovac Quarry, Psunj Mt., Croatia. The white rectangles and circles mark the in-situ laser-ablation track used for U/Pb dating, (ø = 10–15–20 μm), and they are not in scale. Measurement numbers are listed in Table 1.

Fig. 6

Concordia plot of LA-MC-ICP-MS U-Pb zircon analytical results for the PSG-1 sample.
Concordia plot of LA-MC-ICP-MS U-Pb zircon analytical results for the PSG-1 sample.

Fig. 7

Cathodoluminescence images of dated zircon crystals separated from the monzogranite (2PPG-32) from Šandrovac Quarry, Papuk Mt., Croatia. The white rectangles mark the in-situ laser-ablation track used for U/Pb dating, (ø = 10–15 μm) and they are not in scale. Measurement numbers are listed in Table 1.
Cathodoluminescence images of dated zircon crystals separated from the monzogranite (2PPG-32) from Šandrovac Quarry, Papuk Mt., Croatia. The white rectangles mark the in-situ laser-ablation track used for U/Pb dating, (ø = 10–15 μm) and they are not in scale. Measurement numbers are listed in Table 1.

Fig. 8

Concordia plots of LA-MC-ICP-MS U-Pb zircon analytical results (Table 1) for the 2PPG-32 sample.
Concordia plots of LA-MC-ICP-MS U-Pb zircon analytical results (Table 1) for the 2PPG-32 sample.

Fig. 9

Cathodoluminescence images of dated zircon crystals separated from the biotite monzogranite (HEG-31) from Kišeljevac Creek, Papuk Mt., Croatia. The white rectangles mark the in-situ laser-ablation track used for U/Pb dating, (⌀ = 10–15–20 μm), and they are not in scale. Measurement numbers are listed in Table 1.
Cathodoluminescence images of dated zircon crystals separated from the biotite monzogranite (HEG-31) from Kišeljevac Creek, Papuk Mt., Croatia. The white rectangles mark the in-situ laser-ablation track used for U/Pb dating, (⌀ = 10–15–20 μm), and they are not in scale. Measurement numbers are listed in Table 1.

Fig. 10

Concordia plots of LA-MC-ICP-MS U-Pb zircon analytical results (Table 1) for the HEG-31 sample (calculated with a forced upper intercept at 207Pb/206Pb = 0.85 ± 0.05).
Concordia plots of LA-MC-ICP-MS U-Pb zircon analytical results (Table 1) for the HEG-31 sample (calculated with a forced upper intercept at 207Pb/206Pb = 0.85 ± 0.05).

Zircon laser-ablation MC-ICP-MS U-Th-Pb data including the 206Pb/238U minimum ages.

204Pb206Pb207Pb208Pb232Th238U206Pb204Pb$ \frac{^{206}\text{Pb}}{^{204}\text{Pb}} $±2SE207Pb235U$ \frac{^{207}\text{Pb}}{^{235}\text{U}} $±2SE206Pb238U$ \frac{^{206}\text{Pb}}{^{\text{238}}\text{U}} $±Rho 2SE207Pb206Pb$ \frac{^{207}\text{Pb}}{^{206}\text{Pb}} $±2SE208Pb206Pb$ \frac{^{208}\text{Pb}}{^{\text{206}}\text{Pb}} $±2SE208Pb232Th$ \frac{^{208}\text{Pb}}{^{232}\text{Th}} $±2SE238U206Pb$ \frac{^{238}\text{U}}{^{206}\text{Pb}} $±2SE207Pb206Pb$ \frac{^{207}\text{Pb}}{^{\text{206}}\text{Pb}} $±2SE206Pb238U$ \frac{^{206}\text{Pb}}{^{238}\text{U}} $±2SD
Spot #(mV) ×10–6(mV) ×10–3(mV) ×10–4(mV) ×10–4(mV) ×10–2(mV) ×10–1(%)(%)(%)(%)(%)(%)(%)(%)(Ma)
PSG-1
PSG-1_0139_10a1.400.660.490.790.410.1960810.4482.890.06002.770.480.05420.410.3554.540.0191.5516.672.770.05420.41375.610.4
PSG-1_0139_10b3.200.750.580.980.560.23227780.4532.220.06051.840.410.05420.790.3783.850.0172.4616.531.840.05420.79378.77.0
PSG-1_0139_352.203.502.605.202.800.991271630.4812.110.06442.370.560.05410.770.3085.340.0185.8015.532.370.05410.77402.39.5
PSG-1_0139_372.203.902.907.604.301.10208880.4085.680.05465.850.510.05430.290.5303.620.0152.8416.335.850.05430.29342.720
PSG-1_0139_382.202.001.603.201.300.45136320.4211.430.05700.860.300.05400.660.3890.800.0171.1716.550.860.05400.66357.43.1
PSG-1_0139_401.702.301.703.101.800.71168230.4062.560.05372.910.570.05460.310.4043.980.0172.8416.622.910.05460.31337.29.8
PSG-1_0139_521.701.000.751.400.730.2888730.4544.960.06074.940.500.05430.370.3753.520.0183.0216.494.940.05430.37379.918.8
PSG-1_0139_61n.d.0.930.691.300.670.25--0.4694.350.06194.710.540.05440.500.3414.390.0201.8916.154.710.05440.50387.218.2
PSG-1_0139_63n.d.1.401.001.900.960.39--0.4902.490.06443.870.780.05471.210.39618.90.0205.9215.523.870.05471.21402.315.6
2PPG-32
2PPG-32 0140 013.403.102.704.701.200.41
2PPG-32_0140_037.602.102.205.201.200.27132450.4584.760.06102.180.230.05452.386.5492.460.0314.5116.402.180.05452.38381.78.3
2PPG-32_0140_056.606.406.1013.002.900.862095110.4543.790.06061.720.120.05441.455.6572.870.0324.7216.491.720.05441.45379.36.5
2PPG-32_0140_13a5.508.307.307.802.101.001196120.4525.750.06032.600.480.05450.613.5809.320.0408.3516.592.600.05450.61377.49.8
2PPG-32_0140_13b2.905.004.408.602.000.622367100.4504.440.06022.000.560.05421.025.2977.700.0343.3216.622.000.05421.02376.87.5
2PPG-32_0140_153.103.403.005.901.500.45144580.4523.290.05991.480.350.05471.594.5942.240.02625.216.691.480.05471.59375.05.6
2PPG-32_0140_163.102.001.905.801.400.2665170.4484.090.05991.830.730.05431.118.6104.850.0355.1116.691.830.05431.11375.06.9
HEG-31
HEG-31_0137_03a1.902.201.702.501.400.66
31_0137_03b2.709.006.905.002.302.7056802670.44269.80.058761.80.440.05464.910.1491400.02417117.0461.80.05464.91367.7227.2
HEG-31_0137_042.100.410.400.510.120.10942130.56922.30.062215.60.350.06734.260.22527.90.03719.116.0815.60.06734.26389.060.7
HEG-31_0137_052.101.000.790.500.250.30149230.4751.780.06251.850.520.05510.390.1203.140.0202.0615.991.850.05510.39390.87.2
HEG-31_0137_062.302.201.603.801.900.65154560.4662.520.06291.890.370.05430.450.58014.00.01711.015.891.890.05430.45393.27.4
HEG-31_0137_102.101.501.102.701.500.462455400.4576.570.06138.600.650.05404.630.41536.10.0185.2216.318.600.05404.63383.533.0
HEG-31_0137_151.801.100.883.100.830.1676230.7224.260.08634.410.520.06090.660.7935.300.0291.9511.594.410.06090.66533.623.5
HEG-31_0137_16n.d.3.902.903.801.901.20--0.40516.30.054615.00.460.05410.470.26017.80.01723.418.3015.00.05410.47342.751.4
HEG-31_0137_201.902.201.702.100.910.54156010.3882.970.05272.490.420.05390.340.3134.980.0173.4118.962.490.05390.34331.18.2
HEG-31_0137_232.102.001.501.800.990.62117610.4400.580.05840.570.490.05480.280.2011.640.0180.8217.120.570.05480.28365.92.1
HEG-31_0138_051.801.200.901.700.830.28107610.4520.940.06060.870.460.05450.510.4771.960.0171.6116.500.870.05450.51379.33.3
HEG-31_0138_06a1.800.370.310.410.230.0957130.4483.580.05702.240.310.05712.120.2473.530.0175.7117.532.240.05712.12357.48.0
HEG-31_0138_06bn.d.0.830.631.000.490.22--0.4326.010.05725.920.490.05431.600.3468.740.01710.417.495.920.05431.60358.621.2
HEG-31_0138_142.802.402.503.600.800.34272320.5903.150.06641.130.180.06432.020.4111.860.0166.9015.051.130.06432.02414.44.7
HEG-31_0138_192.502.602.004.602.400.781166220.4753.280.06142.370.360.05582.060.7712.050.0183.7816.282.370.05582.06384.19.1
HEG-31_0138_292.800.770.671.200.560.2342920.4932.120.05991.100.260.05941.830.4456.180.0214.8816.691.100.05941.83375.04.1
HEG-31_0138_332.802.201.701.901.900.66180360.4692.260.06132.630.580.05530.760.2313.710.01812.016.322.630.05530.76383.510.1
HEG-31_0138_371.702.201.702.301.300.64148210.4681.290.06241.370.530.05440.190.2944.610.0171.3016.031.370.05440.19390.25.3
HEG-31_0138_402.604.003.103.101.400.97150960.4702.760.06111.720.310.05551.130.1678.520.0193.4916.361.720.05551.13382.36.6
HEG-31_0138_411.701.300.991.100.570.40108610.4221.020.05620.960.470.05450.320.2945.270.0164.2417.790.960.05450.32352.53.4
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