1. bookVolume 8 (2015): Issue 2 (October 2015)
Journal Details
First Published
10 Dec 2012
Publication timeframe
2 times per year
access type Open Access

Recent achievements and applications of solid – phase microextraction in pesticide residues analysis in food

Published Online: 05 Dec 2015
Volume & Issue: Volume 8 (2015) - Issue 2 (October 2015)
Page range: 178 - 190
Journal Details
First Published
10 Dec 2012
Publication timeframe
2 times per year

The current trend in sample preparation methods is devoted to minimizing or eliminating the volume of extractive solvent. In this review, the focus on solid phase microextraction (SPME) as a solvent free sample preparation method for the isolation of pesticides residues in different food matrices is given. To achieve satisfactory extraction efficiency, selection of the fiber coating is an important step in the method development. Here, recent trends in new supporting materials and new fiber coatings development are discussed. Finally, applicability of SPME for the pesticide residues analysis in various food matrices using mainly chromatographic methods is also reviewed.


Abdulrauf LB, Tan GH (2013) Food Chem 141: 4344-4348.10.1016/j.foodchem.2013.07.02223993624Search in Google Scholar

Andraščikova M, Matisova E, Hrouzkova S (2015) Sep Purif Rev 44: 1-18.Search in Google Scholar

Arthur CL, Pawliszyn J (1990) Anal Chem 62: 2145-2148.10.1021/ac00218a019Search in Google Scholar

Bagheri H, Es’haghi A, Es-haghi A, Mesbahi N (2012) Anal Chim Acta 740: 36-42.10.1016/j.aca.2012.06.00122840648Search in Google Scholar

Blasco C, Vazquez-Roig P, Onghena M, Masia A, Pico Y (2011) J Chromatogr A 1218: 4892-4901.10.1016/j.chroma.2011.02.04521411107Search in Google Scholar

Cai L, Gong S, Chen M, Wu C (2006) Anal Chim Acta 559: 89-96.10.1016/j.aca.2005.11.048Search in Google Scholar

Campillo N, Penalver R, Aguinaga N, Hernandez- Cordoba M (2006) Anal Chim Acta 562: 9-15.10.1016/j.aca.2006.01.034Search in Google Scholar

Capobiango HLV, Cardeal ZL (2005) J Braz Chem Soc 16(5): 907-914.10.1590/S0103-50532005000600004Search in Google Scholar

Cardeal ZL, Paes CMD (2006) J Environ Sci Health Part B 41: 369-375.10.1080/0360123060063474516753956Search in Google Scholar

Chai MK, Tan GH (2009) Food Chem 117: 561-567.10.1016/j.foodchem.2009.04.034Search in Google Scholar

Chowdhury MAZ, Fakhruddin ANM, Islam Md.N, Moniruzzaman M, Gan SH, Alam Md.K (2013) Food Control 34: 457-465.10.1016/j.foodcont.2013.05.006Search in Google Scholar

Cortes-Aguado S, Sanchez-Morito N, Arrebola FJ, Garrido Frenich A, Vidal JLM (2008) Food Chem 107: 1314-1325.10.1016/j.foodchem.2007.09.033Search in Google Scholar

Directive 91/414/EEC. Regulation (EC) No 396/2005. Active substances Pesticide EU-MRL. (2005) Off. J. Eur. Union L70: 1.Search in Google Scholar

Djozan D, Ebrahimi B (2008) Anal Chim Acta 616: 152-159.10.1016/j.aca.2008.04.03718482598Search in Google Scholar

Djozan D, Mahkam M, Ebrahimi B (2009) J Chromatogr A, 1216: 2211-2219.10.1016/j.chroma.2008.12.10119185305Search in Google Scholar

Dong C, Zeng Z, Li X (2005) Talanta 66: 721-727.10.1016/j.talanta.2004.12.02018970044Search in Google Scholar

Feng J, Qiu H, Liu X, Jiang S (2013) Trends Anal Chem 46: 44-58.10.1016/j.trac.2013.01.015Search in Google Scholar

Filho AM, Neves dos Santos F, Afonso de Paula Pereira P (2008) Talanta 81: 346-354.Search in Google Scholar

Ghaemi F, Amiri A, Yunus R (2014) Trends Anal Chem 59: 133-143.10.1016/j.trac.2014.04.011Search in Google Scholar

Guillet V, Fave C, Montury M (2009) Journal of Environmental Science and Health Part B 44: 415-422.10.1080/0360123090293458720183044Search in Google Scholar

Heaven MW, Nash D (2012) Food Control 27: 214-227.10.1016/j.foodcont.2012.03.018Search in Google Scholar

Hernández-Borges J, Cifuentes A, Garcia-Montelongo FJ, Rodriguez-Delgado MA (2005) Electrophoresis 26: 980-989. http://ec.europa.eu/sanco_pesticides/public/index.cfm.10.1002/elps.20041032115714540Search in Google Scholar

Hu Y, Yang X, Wang C, Zhao J, Li W, Wang Z (2008) Food Addit Contam 25(3): 314-319.10.1080/0265203070158186418311622Search in Google Scholar

Ibrahim WAW, Farhani H, Sanagi MM, Aboul-Enein HY (2010) J Chromatogr A 1217: 4890-4897.10.1016/j.chroma.2010.05.05020561627Search in Google Scholar

Kataoka H, Ishizaki A, Nonaka Y, Saito K (2009) Anal Chim Acta 655: 8-29.10.1016/j.aca.2009.09.03219925911Search in Google Scholar

Korba K, Pelit L, Pelit FO, Őzdokur KV, Ertaş H, Eroğlu AE, Ertaş FN (2013) J Chromatogr B 929: 90-96.10.1016/j.jchromb.2013.04.02323669608Search in Google Scholar

Kudlejova L, and Risticevic S (2012) Application of Solid- Phase Microextraction in Food and Fragrance Analysis. In Handbook of Solid Phase Microextraction: (Ed) Janusz Pawliszyn, Elsevier, Waterloo, Ontario Canada p 291-334. http://www.sciencedirect.com/science/book/9780124160170.10.1016/B978-0-12-416017-0.00009-7Search in Google Scholar

Kudlejova L, Risticevic S, Vuckovic D (2012) Microextraction Method Development. In Handbook of Solid Phase Microextraction (Ed) Janusz Pawliszyn, Elsevier, Waterloo, Ontario Canada, p 201-249. http://www.sciencedirect.com/science/book/9780124160170.Search in Google Scholar

Luo Y-B, Yuan B-F, Yu, Q-W, Feng Y-Q (2012) J Chromatogr A 1268: 9-15.10.1016/j.chroma.2012.10.03523131764Search in Google Scholar

Mariani MB, Giannetti V, Testani E, Ceccarelli V (2013) J AOAC Int 96(6): 1430-1434.10.5740/jaoacint.11-52924645525Search in Google Scholar

Martins J, Esteves C, Limpo-Faria A, Barros P, Ribeiro N, Simoes T, Correia M, Delerue-Matos C (2012) Food Chem 132: 630-636.10.1016/j.foodchem.2011.10.10226434342Search in Google Scholar

Martins JG, Chavez AA, Waliszewski SM, Cruz AC, Fabila MMG (2013) Chemosphere 92: 233-636.10.1016/j.chemosphere.2013.04.00823648324Search in Google Scholar

Masiá A, Blasco C, Pico Y (2014) Trends Environ Anal Chem 2: 11-24.10.1016/j.teac.2014.03.002Search in Google Scholar

Melo A, Aguiar A, Mansilha C, Pinho O, Ferreira IMPLVO (2012) Food Chem 130: 1090-1097.10.1016/j.foodchem.2011.07.137Search in Google Scholar

Moliner-Martinez Y, Campins-Falco P, Molins-Legua C, Segovia-Martinez L, Seco-Torrecillas A (2009) J Chromatogr A 1216: 6741-6745.10.1016/j.chroma.2009.08.02119709665Search in Google Scholar

Munitz MS, Resnik SL, Montti MIT (2013) Food Chem 136: 1399-1404.10.1016/j.foodchem.2012.09.07923194540Search in Google Scholar

Pereira VL, Fernandes JO, Cunha SC (2014) Trends Food Sci & Technol 36: 96-136.10.1016/j.tifs.2014.01.005Search in Google Scholar

Ramos L (2012) J Chromatogr A, 1221: 84-98.10.1016/j.chroma.2011.11.01122137129Search in Google Scholar

Ravelo-Perez LM, Hernandez-Borges J, Borges-Miquel TM, Rodriguez-Delgado MA (2007) Electrophoresis 28: 4072-4081.10.1002/elps.20070025117957661Search in Google Scholar

Rodrigues FM, Mesquita PRR, Oliveira LS, Oliveira FS, Filho AM, Pereira PAP, Andrade JB (2011) Microchem J 98: 56-61.10.1016/j.microc.2010.11.002Search in Google Scholar

Ruiz del Castillo ML, Rodriguez-Valenciano M, Pena Moreno F, Blanch GP (2012) Talanta 89: 77-83.10.1016/j.talanta.2011.11.06222284462Search in Google Scholar

Sagratini G, Manes J, Giardińa D, Damiani P, Pico Y (2007) J Chromatogr A 1147: 135-143.10.1016/j.chroma.2007.02.06617362971Search in Google Scholar

Sang Z-Y, Wang Y-T, Tsoi Y-K, Leung KS-Y (2013) Food Chem 136: 710-717.10.1016/j.foodchem.2012.08.06023122118Search in Google Scholar

Sapahin HA, Makahleh A, Saad B (2015) Arabian Journal of Chemistry http://dx.doi.org/10.1016/j.arabjc.2014. in Google Scholar

Saraji M, Rezaei B, Boroujeni MK, Bidgoli AAH (2013) J Chromatogr A 1279: 20-26.10.1016/j.chroma.2013.01.01723357752Search in Google Scholar

Song J, Forney CF, Jordan MA (2014) Food Chem 160: 255-259.10.1016/j.foodchem.2014.03.09924799236Search in Google Scholar

Song X-Y, Shi Y-P, Chen J (2013) Food Chem 139: 246-252.10.1016/j.foodchem.2013.01.11223561102Search in Google Scholar

Souza-Silva EA, Lopez-Avila V, Pawliszyn J (2013) J Chromatogr A 1313: 139-146.10.1016/j.chroma.2013.07.07123910603Search in Google Scholar

Tian M, Cheng R, Ye J, Liu X, Jia Q (2014) Food Chem 145: 28-33.10.1016/j.foodchem.2013.08.02924128445Search in Google Scholar

Tranchida PQ, Zoccali M, Schipilliti L, Sciarrone D, Dugo P, Mondello L (2013) J Sep Sci 36: 2145-2150.10.1002/jssc.20120110123576394Search in Google Scholar

Viñas P, Campillo N, Martinez-Castillo N, Hernandez- Cordoba M (2009) J Chromatogr A 1216: 140-146.10.1016/j.chroma.2008.11.03619062028Search in Google Scholar

Wang Y-L, Gao Y-L, Wang P-P, Shang H, Pan S-Y, Li X-J (2013) Talanta 115: 920-927.10.1016/j.talanta.2013.06.05624054683Search in Google Scholar

Wang Y-L, Zeng Z-R, Liu M-M, Yang M, Dong C-Z (2008) Eur Food Res Technol 226: 1091-1098.10.1007/s00217-007-0636-6Search in Google Scholar

Wu F, Lu W, Chen J, Liu W, Zhang L (2010) Talanta 82: 1038-1043.10.1016/j.talanta.2010.06.01620678665Search in Google Scholar

Yang C, Wang J, Li D (2013) Anal Chim Acta 799: 8-22.10.1016/j.aca.2013.07.06924091369Search in Google Scholar

Zhao GY, Wang C, Wu QH, Wang Z (2011) Analytical Method 3: 1410-1417.10.1039/c1ay05099kSearch in Google Scholar

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