Formerly: Beiträge zur Tabakforschung International

Contributions to Tobacco & Nicotine Research

Contributions to Tob. Res.

<abstract>
<title style='display:none'>Abstract</title>
3-Oxo-α-ionol ethyl carbonate, a precursor of megastigmatrienones was prepared by reduction of α-ionone to α-ionol, followed by esterification with ethyl chloroformate and then by oxidation with t-butyl chromate. The total yield was about 23%. Infrared (IR) and mass spectra of this compound were determined. Upon smoking, cigarettes to which 0.002% by weight of the titled compound was added had an improved and more harmonious flavor. The smoke was sweeter and had a cleaner after taste. Experimental results suggest that the title compound added to the tobacco pyrolyzes to form megastigmatrienones during smoking.
</abstract>

Abstract

Research Center of Changsha Cigarette Factory, Changsha, Hunan, China

<article-title>Synthesis of 3-Oxo-α-ionol Ethyl Carbonate and its Conversion to Megastigmatrienones in Tobacco Smoke</article-title>

Synthesis of 3-Oxo-α-ionol Ethyl Carbonate and its Conversion to Megastigmatrienones in Tobacco Smoke

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Advisory Board　　　 Bernhard Eitzinger, delfortgroup AG, Traun, Austria Ernest Groman, University of Vienna, Vienna, Austria Daniel Heck, HeckTox LLC, Greensboro, NC, USA Anne Fisher, University of Kentucky, Lexington, KY, USA Xie Jianping, Zhengzhou Tobacco Research Institute of CNTC, Zhengzhou, China Hubert Klus, St. Pölten, Austria John H. Lauterbach, Lauterbach &amp; Associates LLC, Macon, GA, USA Ramsey Lewis, North Carolina State University, Raleigh, NC, USA Chuan Liu, Southampton, UK Tryggve Ljung, Swedish Match, Stockholm, Sweden Michael W. Ogden, Ogden Ology, LLC, Lewisville, NC, USA Thilo Paschke, Geneva, Switzerland Stephen W. Purkis, Bristol, UK Elmar Richter †, Ludwig-Maximilians-University, Munich, Germany Wolfram Roeper, Hamburg, Germany Wolfgang Trinkies, Bayreuth, Germany Andreas Zemann, Leopold-Franzens-University of Innsbruck, Innsbruck, Austria Editors Wolf-Dieter Heller Gerhard Scherer Editorial Office Barbara Boenke Brigitte Müller Anja Thielen Contact <A href="mailto:editors@beitraege-bti.de">editors@beitraege-bti.de</A> Publisher De Gruyter Poland Bogumiła Zuga 32A Str. 01-811 Warsaw, Poland T: +48 22 701 50 15

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Contributions to Tobacco & Nicotine Research

Synthesis of 3-Oxo-α-ionol Ethyl Carbonate and its Conversion to Megastigmatrienones in Tobacco Smoke

H Yang,
H Yang,
J Liu,
J Liu,
K Li,
K Li,
X Yin,
X Yin,
X Tan and
X Tan and
J Wang
J Wang

Published Online: 30 Dec 2014

Volume & Issue: Volume 19 (2001) - Issue 7 (October 2001)

Page range: 339 - 343

Received: 15 Jan 2001

Accepted: 24 Jul 2001

Journal & Issue Details

Contributions to Tobacco & Nicotine Research

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References

Recent Articles

Contributions to Tobacco & Nicotine Research

Synthesis of 3-Oxo-α-ionol Ethyl Carbonate and its Conversion to Megastigmatrienones in Tobacco Smoke

H Yang,H Yang,J Liu,J Liu,K Li,K Li,X Yin,X Yin,X Tan andX Tan andJ WangJ Wang

Published Online: 30 Dec 2014

Volume & Issue: Volume 19 (2001) - Issue 7 (October 2001)

Page range: 339 - 343

Received: 15 Jan 2001

Accepted: 24 Jul 2001

Journal & Issue Details

Contributions to Tobacco & Nicotine Research

PDF Preview

References

Recent Articles

H Yang,
H Yang,
J Liu,
J Liu,
K Li,
K Li,
X Yin,
X Yin,
X Tan and
X Tan and
J Wang
J Wang